The Use of the Silver Solid Amalgam Electrode for Voltammetric Determination of 9-nitroanthracene

Tomáš Navrátil, Kateřina Nováková, Jiří Barek, Vlastimil Vyskočil, Jaromíra Chýlková

Результат исследований: Материалы для журналаСтатья

5 Цитирования (Scopus)

Выдержка

The voltammetric behavior of 9-nitroanthracene was investigated at a mercury meniscus modified silver solid amalgam electrode (m-AgSAE; inner diameter of 0.5 millimeter) by differential pulse voltammetry (DPV) and adsorptive stripping DPV (DPAdSV). Optimum conditions were found for the determination of this analyte in Britton-Robinson buffer (pH = 10.5): pulse width of 80 milliseconds, pulse height of −50 millivolts, initial potential (Ein) = −100 millivolts, final potential (Efin) = −1200 milivolts, potential of accumulation (Eacc) = −100 millivolts, scan rate of 20 millivolts per second. The limit of detection was found to be 0.7 nanomole per liter (tacc = 60 seconds) by DPAdSV at m-AgSAE. The method was successfully applied for the determination of 9-nitroanthracene in drinking and river water.

Язык оригиналаАнглийский
Страницы (с-по)37-48
Число страниц12
ЖурналAnalytical Letters
Том49
Номер выпуска1
DOI
СостояниеОпубликовано - 2 янв 2016
Опубликовано для внешнего пользованияДа

Отпечаток

Mercury amalgams
Mercury (metal)
Voltammetry
Silver
Electrodes
Rivers
Mercury
Drinking Water
Limit of Detection
Water
Buffers
9-nitroanthracene
Meniscus

ASJC Scopus subject areas

  • Analytical Chemistry
  • Biochemistry
  • Spectroscopy
  • Clinical Biochemistry
  • Biochemistry, medical
  • Electrochemistry

Цитировать

The Use of the Silver Solid Amalgam Electrode for Voltammetric Determination of 9-nitroanthracene. / Navrátil, Tomáš; Nováková, Kateřina; Barek, Jiří; Vyskočil, Vlastimil; Chýlková, Jaromíra.

В: Analytical Letters, Том 49, № 1, 02.01.2016, стр. 37-48.

Результат исследований: Материалы для журналаСтатья

Navrátil, Tomáš ; Nováková, Kateřina ; Barek, Jiří ; Vyskočil, Vlastimil ; Chýlková, Jaromíra. / The Use of the Silver Solid Amalgam Electrode for Voltammetric Determination of 9-nitroanthracene. В: Analytical Letters. 2016 ; Том 49, № 1. стр. 37-48.
@article{e574f08291ec498b841bb5ee44a8182f,
title = "The Use of the Silver Solid Amalgam Electrode for Voltammetric Determination of 9-nitroanthracene",
abstract = "The voltammetric behavior of 9-nitroanthracene was investigated at a mercury meniscus modified silver solid amalgam electrode (m-AgSAE; inner diameter of 0.5 millimeter) by differential pulse voltammetry (DPV) and adsorptive stripping DPV (DPAdSV). Optimum conditions were found for the determination of this analyte in Britton-Robinson buffer (pH = 10.5): pulse width of 80 milliseconds, pulse height of −50 millivolts, initial potential (Ein) = −100 millivolts, final potential (Efin) = −1200 milivolts, potential of accumulation (Eacc) = −100 millivolts, scan rate of 20 millivolts per second. The limit of detection was found to be 0.7 nanomole per liter (tacc = 60 seconds) by DPAdSV at m-AgSAE. The method was successfully applied for the determination of 9-nitroanthracene in drinking and river water.",
keywords = "9-Nitroanthracene, silver solid amalgam electrode, voltammetry",
author = "Tom{\'a}š Navr{\'a}til and Kateřina Nov{\'a}kov{\'a} and Jiř{\'i} Barek and Vlastimil Vyskočil and Jarom{\'i}ra Ch{\'y}lkov{\'a}",
year = "2016",
month = "1",
day = "2",
doi = "10.1080/00032719.2014.979295",
language = "English",
volume = "49",
pages = "37--48",
journal = "Analytical Letters",
issn = "0003-2719",
publisher = "Taylor and Francis Ltd.",
number = "1",

}

TY - JOUR

T1 - The Use of the Silver Solid Amalgam Electrode for Voltammetric Determination of 9-nitroanthracene

AU - Navrátil, Tomáš

AU - Nováková, Kateřina

AU - Barek, Jiří

AU - Vyskočil, Vlastimil

AU - Chýlková, Jaromíra

PY - 2016/1/2

Y1 - 2016/1/2

N2 - The voltammetric behavior of 9-nitroanthracene was investigated at a mercury meniscus modified silver solid amalgam electrode (m-AgSAE; inner diameter of 0.5 millimeter) by differential pulse voltammetry (DPV) and adsorptive stripping DPV (DPAdSV). Optimum conditions were found for the determination of this analyte in Britton-Robinson buffer (pH = 10.5): pulse width of 80 milliseconds, pulse height of −50 millivolts, initial potential (Ein) = −100 millivolts, final potential (Efin) = −1200 milivolts, potential of accumulation (Eacc) = −100 millivolts, scan rate of 20 millivolts per second. The limit of detection was found to be 0.7 nanomole per liter (tacc = 60 seconds) by DPAdSV at m-AgSAE. The method was successfully applied for the determination of 9-nitroanthracene in drinking and river water.

AB - The voltammetric behavior of 9-nitroanthracene was investigated at a mercury meniscus modified silver solid amalgam electrode (m-AgSAE; inner diameter of 0.5 millimeter) by differential pulse voltammetry (DPV) and adsorptive stripping DPV (DPAdSV). Optimum conditions were found for the determination of this analyte in Britton-Robinson buffer (pH = 10.5): pulse width of 80 milliseconds, pulse height of −50 millivolts, initial potential (Ein) = −100 millivolts, final potential (Efin) = −1200 milivolts, potential of accumulation (Eacc) = −100 millivolts, scan rate of 20 millivolts per second. The limit of detection was found to be 0.7 nanomole per liter (tacc = 60 seconds) by DPAdSV at m-AgSAE. The method was successfully applied for the determination of 9-nitroanthracene in drinking and river water.

KW - 9-Nitroanthracene

KW - silver solid amalgam electrode

KW - voltammetry

UR - http://www.scopus.com/inward/record.url?scp=84944937745&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=84944937745&partnerID=8YFLogxK

U2 - 10.1080/00032719.2014.979295

DO - 10.1080/00032719.2014.979295

M3 - Article

AN - SCOPUS:84944937745

VL - 49

SP - 37

EP - 48

JO - Analytical Letters

JF - Analytical Letters

SN - 0003-2719

IS - 1

ER -