The Hydrothermal Synthesis Duration Influence on Calcium Phosphate and Hydroxyapatite Phase Composition

Аннотация

This paper reports the hydrothermal synthesis process duration influence on phase composition, crystallinity degree, morphology and dispersity of the hydroxyapatite powder. The calcium phosphate and hydroxyapatite were synthesized in precursor system Ca(NO₃)_2-(NH₄)₂HPO₄-NH₄OH. The obtained powders were characterized with X - Ray diffraction, Fourier Transform spectroscopy (FTIR) and Raman spectroscopy. The results demonstrate: the increasing of the synthesis time duration has no influence on the phase composition. However, the synthesis duration time growth from 12 to 48 hours make possible increase the crystallinity degree from 0.68 to 0.98.

Язык оригинала	Английский
Номер статьи	012024
Журнал	IOP Conference Series: Materials Science and Engineering
Том	731
Номер выпуска	1
DOI	https://doi.org/10.1088/1757-899X/731/1/012024
Состояние	Опубликовано - 20 янв 2020
Событие	International Science and Technology Conference for Youth on Advanced Materials for Engineering and Medicine, AMEM 2019 - Tomsk, Российская Федерация Продолжительность: 30 сен 2019 → 5 окт 2019

ASJC Scopus subject areas

Materials Science(all)
Engineering(all)

Доступ к документу

10.1088/1757-899X/731/1/012024

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Цитировать

The Hydrothermal Synthesis Duration Influence on Calcium Phosphate and Hydroxyapatite Phase Composition. / Chuprunov, K.; Yudin, A.; Leybo, D.; Lysov, D.; Kolesnikov, E.; Kuznetsov, D.; Godymchuk, A.; Mandal, A. R.

В: IOP Conference Series: Materials Science and Engineering, Том 731, № 1, 012024, 20.01.2020.

Результат исследований: Материалы для журнала › рецензирование

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abstract = "This paper reports the hydrothermal synthesis process duration influence on phase composition, crystallinity degree, morphology and dispersity of the hydroxyapatite powder. The calcium phosphate and hydroxyapatite were synthesized in precursor system Ca(NO3)2-(NH4)2HPO4-NH4OH. The obtained powders were characterized with X - Ray diffraction, Fourier Transform spectroscopy (FTIR) and Raman spectroscopy. The results demonstrate: the increasing of the synthesis time duration has no influence on the phase composition. However, the synthesis duration time growth from 12 to 48 hours make possible increase the crystallinity degree from 0.68 to 0.98.",

author = "K. Chuprunov and A. Yudin and D. Leybo and D. Lysov and E. Kolesnikov and D. Kuznetsov and A. Godymchuk and Mandal, {A. R.}",

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T1 - The Hydrothermal Synthesis Duration Influence on Calcium Phosphate and Hydroxyapatite Phase Composition

AU - Chuprunov, K.

AU - Yudin, A.

AU - Leybo, D.

AU - Lysov, D.

AU - Kolesnikov, E.

AU - Kuznetsov, D.

AU - Godymchuk, A.

AU - Mandal, A. R.

PY - 2020/1/20

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N2 - This paper reports the hydrothermal synthesis process duration influence on phase composition, crystallinity degree, morphology and dispersity of the hydroxyapatite powder. The calcium phosphate and hydroxyapatite were synthesized in precursor system Ca(NO3)2-(NH4)2HPO4-NH4OH. The obtained powders were characterized with X - Ray diffraction, Fourier Transform spectroscopy (FTIR) and Raman spectroscopy. The results demonstrate: the increasing of the synthesis time duration has no influence on the phase composition. However, the synthesis duration time growth from 12 to 48 hours make possible increase the crystallinity degree from 0.68 to 0.98.

AB - This paper reports the hydrothermal synthesis process duration influence on phase composition, crystallinity degree, morphology and dispersity of the hydroxyapatite powder. The calcium phosphate and hydroxyapatite were synthesized in precursor system Ca(NO3)2-(NH4)2HPO4-NH4OH. The obtained powders were characterized with X - Ray diffraction, Fourier Transform spectroscopy (FTIR) and Raman spectroscopy. The results demonstrate: the increasing of the synthesis time duration has no influence on the phase composition. However, the synthesis duration time growth from 12 to 48 hours make possible increase the crystallinity degree from 0.68 to 0.98.

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