Synthesis and characterization of LiClO4 center dot H2O

S. I. Ivlev, Dmitry Vasilievich Akimov, N. B. Egorov, F. Kraus

Отделение ядерно-топливного цикла

Результат исследований: Материалы для журнала › Статья

Аннотация

Lithium perchlorate monohydrate was synthesized and characterized. The compound crystallizes isotypic to sodium perchlorate monohydrate in the monoclinic space group type C2/c with a = 14.2592(6) Å, b = 5.2921(2) Å, c = 10.3382(4) Å, β = 111.765(2)°, V = 724.52(5) Å³, Z = 8, at T = 110 K. Additionally, we investigated the compound by means of IR and Raman spectroscopy, powder X-ray diffraction, thermal analysis (TG/DSC), and solid-state computational calculations.

Язык оригинала	Английский
Страницы (с-по)	279-288
Число страниц	10
Журнал	Monatshefte fur Chemie
Том	147
Номер выпуска	2
DOI	https://doi.org/10.1007/s00706-015-1603-8
Состояние	Опубликовано - фев 2016

ASJC Scopus subject areas

Chemistry(all)

Доступ к документу

10.1007/s00706-015-1603-8

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Ivlev, S. I., Akimov, D. V., Egorov, N. B., & Kraus, F. (2016). Synthesis and characterization of LiClO4 center dot H2O. Monatshefte fur Chemie, 147(2), 279-288. https://doi.org/10.1007/s00706-015-1603-8

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title = "Synthesis and characterization of LiClO4 center dot H2O",

abstract = "Lithium perchlorate monohydrate was synthesized and characterized. The compound crystallizes isotypic to sodium perchlorate monohydrate in the monoclinic space group type C2/c with a = 14.2592(6) {\AA}, b = 5.2921(2) {\AA}, c = 10.3382(4) {\AA}, β = 111.765(2)°, V = 724.52(5) {\AA}3, Z = 8, at T = 110 K. Additionally, we investigated the compound by means of IR and Raman spectroscopy, powder X-ray diffraction, thermal analysis (TG/DSC), and solid-state computational calculations.",

keywords = "DFT calculations, IR spectra, Lithium, Perchlorate, Raman spectra, Single crystal diffraction",

author = "Ivlev, {S. I.} and Akimov, {Dmitry Vasilievich} and Egorov, {N. B.} and F. Kraus",

year = "2016",

month = feb,

doi = "10.1007/s00706-015-1603-8",

language = "English",

volume = "147",

pages = "279--288",

journal = "Monatshefte fur Chemie",

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TY - JOUR

T1 - Synthesis and characterization of LiClO4 center dot H2O

AU - Ivlev, S. I.

AU - Akimov, Dmitry Vasilievich

AU - Egorov, N. B.

AU - Kraus, F.

PY - 2016/2

Y1 - 2016/2

N2 - Lithium perchlorate monohydrate was synthesized and characterized. The compound crystallizes isotypic to sodium perchlorate monohydrate in the monoclinic space group type C2/c with a = 14.2592(6) Å, b = 5.2921(2) Å, c = 10.3382(4) Å, β = 111.765(2)°, V = 724.52(5) Å3, Z = 8, at T = 110 K. Additionally, we investigated the compound by means of IR and Raman spectroscopy, powder X-ray diffraction, thermal analysis (TG/DSC), and solid-state computational calculations.

AB - Lithium perchlorate monohydrate was synthesized and characterized. The compound crystallizes isotypic to sodium perchlorate monohydrate in the monoclinic space group type C2/c with a = 14.2592(6) Å, b = 5.2921(2) Å, c = 10.3382(4) Å, β = 111.765(2)°, V = 724.52(5) Å3, Z = 8, at T = 110 K. Additionally, we investigated the compound by means of IR and Raman spectroscopy, powder X-ray diffraction, thermal analysis (TG/DSC), and solid-state computational calculations.

KW - DFT calculations

KW - IR spectra

KW - Lithium

KW - Perchlorate

KW - Raman spectra

KW - Single crystal diffraction

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