TY - JOUR
T1 - Synthesis and characterization of LiClO4 center dot H2O
AU - Ivlev, S. I.
AU - Akimov, Dmitry Vasilievich
AU - Egorov, N. B.
AU - Kraus, F.
PY - 2016/2
Y1 - 2016/2
N2 - Lithium perchlorate monohydrate was synthesized and characterized. The compound crystallizes isotypic to sodium perchlorate monohydrate in the monoclinic space group type C2/c with a = 14.2592(6) Å, b = 5.2921(2) Å, c = 10.3382(4) Å, β = 111.765(2)°, V = 724.52(5) Å3, Z = 8, at T = 110 K. Additionally, we investigated the compound by means of IR and Raman spectroscopy, powder X-ray diffraction, thermal analysis (TG/DSC), and solid-state computational calculations.
AB - Lithium perchlorate monohydrate was synthesized and characterized. The compound crystallizes isotypic to sodium perchlorate monohydrate in the monoclinic space group type C2/c with a = 14.2592(6) Å, b = 5.2921(2) Å, c = 10.3382(4) Å, β = 111.765(2)°, V = 724.52(5) Å3, Z = 8, at T = 110 K. Additionally, we investigated the compound by means of IR and Raman spectroscopy, powder X-ray diffraction, thermal analysis (TG/DSC), and solid-state computational calculations.
KW - DFT calculations
KW - IR spectra
KW - Lithium
KW - Perchlorate
KW - Raman spectra
KW - Single crystal diffraction
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U2 - 10.1007/s00706-015-1603-8
DO - 10.1007/s00706-015-1603-8
M3 - Article
AN - SCOPUS:84957430991
VL - 147
SP - 279
EP - 288
JO - Monatshefte fur Chemie
JF - Monatshefte fur Chemie
SN - 0026-9247
IS - 2
ER -