Recrystallization and formation of spheroidal gold particles in amorphous-like AlN–TiB2–TiSi2 coatings after annealing and subsequent implantation

A. D. Pogrebnjak, A. A. Dem’yanenko, V. M. Beresnev, O. V. Sobol’, O. M. Ivasishin, K. Oyoshi, Y. Takeda, H. Amekura, A. I. Kupchishin

Результат исследований: Материалы для журналаСтатья

Выдержка

The recrystallization of the structure of an X-ray amorphous AlN–TiB2–TiSi2 coating containing short-range order regions with characteristic sizes of 0.8–1.0 nm has been performed using a negative gold ion (Au) beam and high-temperature annealing. Direct measurements using methods of high-resolution transmission electron microscopy (HRTEM) and energy-dispersive X-ray spectral (EDXS) microanalysis have demonstrated that thermal annealing at a temperature of 1300°C in air results in the formation of nanoscale (10–15 nm) phases AlN, AlB2, Al3O3, and TiO2, whereas the ion implantation of negative ions Au leads to a fragmentation (decrease in the size) of nanograins to 2–5 nm with the formation of spheroidal gold nanocrystallites a few nanometers in size, as well as to the formation of an amorphous oxide film in the depth (near-surface layer) of the coating due to ballistic ion mixing and collision cascades.

Язык оригиналаАнглийский
Страницы (с-по)1453-1457
Число страниц5
ЖурналPhysics of the Solid State
Том58
Номер выпуска7
DOI
СостояниеОпубликовано - 1 июл 2016
Опубликовано для внешнего пользованияДа

Отпечаток

Gold
implantation
Annealing
gold
coatings
X rays
Coatings
Nanocrystallites
annealing
Microanalysis
Amorphous films
Ballistics
High resolution transmission electron microscopy
Ion implantation
Ion beams
Oxide films
Negative ions
Ions
microanalysis
negative ions

ASJC Scopus subject areas

  • Electronic, Optical and Magnetic Materials
  • Condensed Matter Physics

Цитировать

Recrystallization and formation of spheroidal gold particles in amorphous-like AlN–TiB2–TiSi2 coatings after annealing and subsequent implantation. / Pogrebnjak, A. D.; Dem’yanenko, A. A.; Beresnev, V. M.; Sobol’, O. V.; Ivasishin, O. M.; Oyoshi, K.; Takeda, Y.; Amekura, H.; Kupchishin, A. I.

В: Physics of the Solid State, Том 58, № 7, 01.07.2016, стр. 1453-1457.

Результат исследований: Материалы для журналаСтатья

Pogrebnjak, AD, Dem’yanenko, AA, Beresnev, VM, Sobol’, OV, Ivasishin, OM, Oyoshi, K, Takeda, Y, Amekura, H & Kupchishin, AI 2016, 'Recrystallization and formation of spheroidal gold particles in amorphous-like AlN–TiB2–TiSi2 coatings after annealing and subsequent implantation', Physics of the Solid State, том. 58, № 7, стр. 1453-1457. https://doi.org/10.1134/S1063783416070283
Pogrebnjak, A. D. ; Dem’yanenko, A. A. ; Beresnev, V. M. ; Sobol’, O. V. ; Ivasishin, O. M. ; Oyoshi, K. ; Takeda, Y. ; Amekura, H. ; Kupchishin, A. I. / Recrystallization and formation of spheroidal gold particles in amorphous-like AlN–TiB2–TiSi2 coatings after annealing and subsequent implantation. В: Physics of the Solid State. 2016 ; Том 58, № 7. стр. 1453-1457.
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AU - Beresnev, V. M.

AU - Sobol’, O. V.

AU - Ivasishin, O. M.

AU - Oyoshi, K.

AU - Takeda, Y.

AU - Amekura, H.

AU - Kupchishin, A. I.

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N2 - The recrystallization of the structure of an X-ray amorphous AlN–TiB2–TiSi2 coating containing short-range order regions with characteristic sizes of 0.8–1.0 nm has been performed using a negative gold ion (Au–) beam and high-temperature annealing. Direct measurements using methods of high-resolution transmission electron microscopy (HRTEM) and energy-dispersive X-ray spectral (EDXS) microanalysis have demonstrated that thermal annealing at a temperature of 1300°C in air results in the formation of nanoscale (10–15 nm) phases AlN, AlB2, Al3O3, and TiO2, whereas the ion implantation of negative ions Au– leads to a fragmentation (decrease in the size) of nanograins to 2–5 nm with the formation of spheroidal gold nanocrystallites a few nanometers in size, as well as to the formation of an amorphous oxide film in the depth (near-surface layer) of the coating due to ballistic ion mixing and collision cascades.

AB - The recrystallization of the structure of an X-ray amorphous AlN–TiB2–TiSi2 coating containing short-range order regions with characteristic sizes of 0.8–1.0 nm has been performed using a negative gold ion (Au–) beam and high-temperature annealing. Direct measurements using methods of high-resolution transmission electron microscopy (HRTEM) and energy-dispersive X-ray spectral (EDXS) microanalysis have demonstrated that thermal annealing at a temperature of 1300°C in air results in the formation of nanoscale (10–15 nm) phases AlN, AlB2, Al3O3, and TiO2, whereas the ion implantation of negative ions Au– leads to a fragmentation (decrease in the size) of nanograins to 2–5 nm with the formation of spheroidal gold nanocrystallites a few nanometers in size, as well as to the formation of an amorphous oxide film in the depth (near-surface layer) of the coating due to ballistic ion mixing and collision cascades.

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