Phase composition and pore structure of nanoparticulate tin oxides prepared by AC electrochemical synthesis

V. V. Korobochkin, M. A. Balmashnov, D. A. Gorlushko, Natalia Vasilievna Usoltseva, V. V. Bochkareva

Научно-образовательный центр Н.М.Кижнера

Результат исследований: Материалы для журнала › Статья

Аннотация

The effect of current density and sodium chloride concentration in solution on the phase composition and pore structure of the products of ac electrolysis of metallic Sn has been studied using X-ray diffraction, thermogravimetry, differential scanning calorimetry, electron microscopy, and low-temperature nitrogen adsorption measurements. The results demonstrate that the synthesis products consist of tin(II) and tin(IV) oxides and hydroxides, whose percentages depend on electrolysis conditions, and have a large specific surface area and mesoporous structure. The average particle size ranges from 10 to 30 nm.

Язык оригинала	Английский
Страницы (с-по)	993-999
Число страниц	7
Журнал	Inorganic Materials
Том	49
Номер выпуска	10
DOI	https://doi.org/10.1134/S0020168513100051
Состояние	Опубликовано - окт 2013

ASJC Scopus subject areas

Inorganic Chemistry
Chemical Engineering(all)
Materials Chemistry
Metals and Alloys

Доступ к документу

10.1134/S0020168513100051

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Цитировать

Korobochkin, V. V., Balmashnov, M. A., Gorlushko, D. A., Usoltseva, N. V., & Bochkareva, V. V. (2013). Phase composition and pore structure of nanoparticulate tin oxides prepared by AC electrochemical synthesis. Inorganic Materials, 49(10), 993-999. https://doi.org/10.1134/S0020168513100051

Phase composition and pore structure of nanoparticulate tin oxides prepared by AC electrochemical synthesis. / Korobochkin, V. V.; Balmashnov, M. A.; Gorlushko, D. A.; Usoltseva, Natalia Vasilievna; Bochkareva, V. V.

В: Inorganic Materials, Том 49, № 10, 10.2013, стр. 993-999.

Результат исследований: Материалы для журнала › Статья

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AU - Gorlushko, D. A.

AU - Usoltseva, Natalia Vasilievna

AU - Bochkareva, V. V.

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AB - The effect of current density and sodium chloride concentration in solution on the phase composition and pore structure of the products of ac electrolysis of metallic Sn has been studied using X-ray diffraction, thermogravimetry, differential scanning calorimetry, electron microscopy, and low-temperature nitrogen adsorption measurements. The results demonstrate that the synthesis products consist of tin(II) and tin(IV) oxides and hydroxides, whose percentages depend on electrolysis conditions, and have a large specific surface area and mesoporous structure. The average particle size ranges from 10 to 30 nm.

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