Phase composition and pore structure of nanoparticulate tin oxides prepared by AC electrochemical synthesis

V. V. Korobochkin, M. A. Balmashnov, D. A. Gorlushko, Natalia Vasilievna Usoltseva, V. V. Bochkareva

Результат исследований: Материалы для журналаСтатья

2 Цитирования (Scopus)

Аннотация

The effect of current density and sodium chloride concentration in solution on the phase composition and pore structure of the products of ac electrolysis of metallic Sn has been studied using X-ray diffraction, thermogravimetry, differential scanning calorimetry, electron microscopy, and low-temperature nitrogen adsorption measurements. The results demonstrate that the synthesis products consist of tin(II) and tin(IV) oxides and hydroxides, whose percentages depend on electrolysis conditions, and have a large specific surface area and mesoporous structure. The average particle size ranges from 10 to 30 nm.

Язык оригиналаАнглийский
Страницы (с-по)993-999
Число страниц7
ЖурналInorganic Materials
Том49
Номер выпуска10
DOI
СостояниеОпубликовано - окт 2013

ASJC Scopus subject areas

  • Inorganic Chemistry
  • Chemical Engineering(all)
  • Materials Chemistry
  • Metals and Alloys

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