m-Iodosylbenzoic acid, a tagged hypervalent iodine reagent for the iodo-functionalization of alkenes and alkynes

Mekhman S. Yusubov, Roza Ya Yusubova, Andreas Kirschning, Joo Yeon Park, Ki Whan Chi

Результат исследований: Материалы для журналаСтатья

25 Цитирования (Scopus)

Выдержка

An efficient and facile method for the iodo-functionalization of alkenes 5 and alkynes 6 by using recyclable m-iodosylbenzoic acid (2) was developed. The final products can be easily isolated without any chromatographic purification by simple treatment of the crude mixture with an anionic exchange resin. Unreacted m-iodosylbenzoic acid and reduced m-iodobenzoic acid are effectively recovered from the resin by acidification with hydrochloric acid.

Язык оригиналаАнглийский
Страницы (с-по)1506-1509
Число страниц4
ЖурналTetrahedron Letters
Том49
Номер выпуска9
DOI
СостояниеОпубликовано - 25 фев 2008

Отпечаток

Iodobenzoates
Alkynes
Hydrochloric Acid
Alkenes
Iodine
Resins
Acids
Acidification
Purification
2-iodosobenzoic acid

ASJC Scopus subject areas

  • Biochemistry
  • Drug Discovery
  • Organic Chemistry

Цитировать

m-Iodosylbenzoic acid, a tagged hypervalent iodine reagent for the iodo-functionalization of alkenes and alkynes. / Yusubov, Mekhman S.; Yusubova, Roza Ya; Kirschning, Andreas; Park, Joo Yeon; Chi, Ki Whan.

В: Tetrahedron Letters, Том 49, № 9, 25.02.2008, стр. 1506-1509.

Результат исследований: Материалы для журналаСтатья

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AU - Yusubova, Roza Ya

AU - Kirschning, Andreas

AU - Park, Joo Yeon

AU - Chi, Ki Whan

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KW - Hypervalent iodine

KW - Iodination

KW - m-Iodosobenzoic acid

KW - Scavenger

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