Hydrogen calibration of GD-spectrometer using Zr-1Nb alloy

Andrey A. Mikhaylov, Tatiana S. Priamushko, Maria N. Babikhina, Victor N. Kudiiarov, Rene Heller, Roman S. Laptev, Andrey M. Lider

Результат исследований: Материалы для журналаСтатьярецензирование

2 Цитирования (Scopus)

Аннотация

To study the hydrogen distribution in Zr-1Nb alloy (E(cyrillic)110 alloy) GD-OES was applied in this work. Qualitative analysis needs the standard samples with hydrogen. However, the standard samples with high concentrations of hydrogen in the zirconium alloy which would meet the requirements of the shape, size are absent. In this work method of Zr + H calibration samples production was performed at the first time. Automated Complex Gas Reaction Controller was used for samples hydrogenation. To calculate the parameters of post-hydrogenation incubation of the samples in an inert gas atmosphere the diffusion equations were used. Absolute hydrogen concentrations in the samples were determined by melting in the inert gas atmosphere using RHEN602 analyzer (LECO Company). Hydrogen distribution was studied using nuclear reaction analysis (HZDR, Dresden, Germany). RF GD-OES was used for calibration. The depth of the craters was measured with the help of a Hommel-Etamic profilometer by Jenoptik, Germany.

Язык оригиналаАнглийский
ЖурналApplied Surface Science
DOI
СостояниеПринято/в печати - 31 окт 2016

ASJC Scopus subject areas

  • Surfaces, Coatings and Films

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