High resolution NMR of free radicals: <sup>13</sup>C magic angle spinning of two solid organic free radicals derived from 4,5-dihydro-1H-imidazol-3-oxide- 1-oxyl and theoretical calculation of their NMR properties

Аннотация

The ¹³C CPMAS NMR spectra of two 4,4,5,5-tetramethyl-2-(1H- and 2H-pyrazol-3-yl)-2-imidazoline-1-oxyl-3-oxides have been recorded and their signals assigned, through unrestricted density functional theory (UDFT) calculations of their absolute shieldings, with satisfactory results.

Язык оригинала	Английский
Страницы (с-по)	114-127
Число страниц	14
Журнал	Arkivoc
Том	2011
Номер выпуска	3
Состояние	Опубликовано - 26 дек 2010
Опубликовано для внешнего пользования	Да

ASJC Scopus subject areas

Organic Chemistry

Доступ к документу

Fingerprint Подробные сведения о темах исследования «High resolution NMR of free radicals: <sup>13</sup>C magic angle spinning of two solid organic free radicals derived from 4,5-dihydro-1H-imidazol-3-oxide- 1-oxyl and theoretical calculation of their NMR properties». Вместе они формируют уникальный семантический отпечаток (fingerprint).

Цитировать

María, D. S., Claramunt, R. M., Vasilevsky, S. F., Klyatskaya, S. V., Alkorta, I., & Elguero, J. (2010). High resolution NMR of free radicals: ¹³C magic angle spinning of two solid organic free radicals derived from 4,5-dihydro-1H-imidazol-3-oxide- 1-oxyl and theoretical calculation of their NMR properties. Arkivoc, 2011(3), 114-127.

High resolution NMR of free radicals : ¹³C magic angle spinning of two solid organic free radicals derived from 4,5-dihydro-1H-imidazol-3-oxide- 1-oxyl and theoretical calculation of their NMR properties. / María, Dolores Santa; Claramunt, Rosa M.; Vasilevsky, Sergey F.; Klyatskaya, Svetlana V.; Alkorta, Ibon; Elguero, José.

В: Arkivoc, Том 2011, № 3, 26.12.2010, стр. 114-127.

Результат исследований: Материалы для журнала › Статья

María, Dolores Santa ; Claramunt, Rosa M. ; Vasilevsky, Sergey F. ; Klyatskaya, Svetlana V. ; Alkorta, Ibon ; Elguero, José. / High resolution NMR of free radicals : ¹³C magic angle spinning of two solid organic free radicals derived from 4,5-dihydro-1H-imidazol-3-oxide- 1-oxyl and theoretical calculation of their NMR properties. В: Arkivoc. 2010 ; Том 2011, № 3. стр. 114-127.

@article{0f572b8be0dc46419ad1631cc736e362,

title = "High resolution NMR of free radicals: 13C magic angle spinning of two solid organic free radicals derived from 4,5-dihydro-1H-imidazol-3-oxide- 1-oxyl and theoretical calculation of their NMR properties",

abstract = "The 13C CPMAS NMR spectra of two 4,4,5,5-tetramethyl-2-(1H- and 2H-pyrazol-3-yl)-2-imidazoline-1-oxyl-3-oxides have been recorded and their signals assigned, through unrestricted density functional theory (UDFT) calculations of their absolute shieldings, with satisfactory results.",

keywords = "GIAO, Nitronylnitroxide radicals, P)",

author = "Mar{\'i}a, {Dolores Santa} and Claramunt, {Rosa M.} and Vasilevsky, {Sergey F.} and Klyatskaya, {Svetlana V.} and Ibon Alkorta and Jos{\'e} Elguero",

year = "2010",

month = dec,

day = "26",

language = "English",

volume = "2011",

pages = "114--127",

journal = "Arkivoc",

issn = "1424-6376",

publisher = "Arkat USA",

number = "3",

}

TY - JOUR

T1 - High resolution NMR of free radicals

T2 - 13C magic angle spinning of two solid organic free radicals derived from 4,5-dihydro-1H-imidazol-3-oxide- 1-oxyl and theoretical calculation of their NMR properties

AU - María, Dolores Santa

AU - Claramunt, Rosa M.

AU - Vasilevsky, Sergey F.

AU - Klyatskaya, Svetlana V.

AU - Alkorta, Ibon

AU - Elguero, José

PY - 2010/12/26

Y1 - 2010/12/26

N2 - The 13C CPMAS NMR spectra of two 4,4,5,5-tetramethyl-2-(1H- and 2H-pyrazol-3-yl)-2-imidazoline-1-oxyl-3-oxides have been recorded and their signals assigned, through unrestricted density functional theory (UDFT) calculations of their absolute shieldings, with satisfactory results.

AB - The 13C CPMAS NMR spectra of two 4,4,5,5-tetramethyl-2-(1H- and 2H-pyrazol-3-yl)-2-imidazoline-1-oxyl-3-oxides have been recorded and their signals assigned, through unrestricted density functional theory (UDFT) calculations of their absolute shieldings, with satisfactory results.

KW - GIAO

KW - Nitronylnitroxide radicals

KW - P)

UR - http://www.scopus.com/inward/record.url?scp=79953080431&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=79953080431&partnerID=8YFLogxK

M3 - Article

AN - SCOPUS:79953080431

VL - 2011

SP - 114

EP - 127

JO - Arkivoc

JF - Arkivoc

SN - 1424-6376

IS - 3

ER -