4-Iodoantipyrine synthesized by means of solid-state mechanical activation

E. A. Krasnokutskaya, M. E. Trusova, N. S. Gibert, V. D. Filimonov

Результат исследований: Материалы для журнала › Статья › рецензирование

Аннотация

Antipyrine and its benzenesulfonate were iodinated by solid-state mechanical activation (in the absence of solvent) under the action of iodine, iodine chloride, Me₄N⁺ICl₂ ^-, and Et₄N⁺ICl₂ ^- with the formation of 4-iodoantipyrine. The proposed process does not require organic solvents and meets all Green Chemistry demands. The best results were achieved with the use of tetraalkylammonium salts Me₄N⁺ICl₂ ^- and Et₄N⁺ICl₂ ^-.

Язык оригинала	Английский
Страницы (с-по)	154-156
Число страниц	3
Журнал	Pharmaceutical Chemistry Journal
Том	41
Номер выпуска	3
DOI	https://doi.org/10.1007/s11094-007-0034-1
Состояние	Опубликовано - мар 2007

ASJC Scopus subject areas

Molecular Medicine
Pharmacology, Toxicology and Pharmaceutics(all)

Доступ к документу

10.1007/s11094-007-0034-1

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author = "Krasnokutskaya, {E. A.} and Trusova, {M. E.} and Gibert, {N. S.} and Filimonov, {V. D.}",

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AU - Krasnokutskaya, E. A.

AU - Trusova, M. E.

AU - Gibert, N. S.

AU - Filimonov, V. D.

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AB - Antipyrine and its benzenesulfonate were iodinated by solid-state mechanical activation (in the absence of solvent) under the action of iodine, iodine chloride, Me4N+ICl2 -, and Et4N+ICl2 - with the formation of 4-iodoantipyrine. The proposed process does not require organic solvents and meets all Green Chemistry demands. The best results were achieved with the use of tetraalkylammonium salts Me4N+ICl2 - and Et4N+ICl2 -.

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