Validation of a method for assay of sulfur hexafluoride in a new contrast agent by gas chromatography

S. V. Krivoshchekov, M. S. Lar’kina, S. S. Vlasov, L. A. Drygunova, A. M. Gur’ev, M. V. Belousov, M. S. Yusubov

Research School of Chemistry & Applied Biomedical Sciences

Research output: Contribution to journal › Article

Abstract

A method for assaying sulfur hexafluoride in a new contrast agent by gas chromatography is described. Detection was with an electron capture detector (ECD). Sulfur hexafluoride was extracted from samples using heptane as the solvent. The method was validated in terms of the following parameters: specificity, linearity, correctness, stability, and inter-and intralaboratory precision.

Original language	English
Pages (from-to)	222-225
Number of pages	4
Journal	Pharmaceutical Chemistry Journal
Volume	51
Issue number	3
DOIs	https://doi.org/10.1007/s11094-017-1586-3
Publication status	Published - 1 Jan 2017

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Keywords

Assay
Gas chromatography
Sulfur hexafluoride

ASJC Scopus subject areas

Pharmacology
Drug Discovery

Cite this

Krivoshchekov, S. V., Lar’kina, M. S., Vlasov, S. S., Drygunova, L. A., Gur’ev, A. M., Belousov, M. V., & Yusubov, M. S. (2017). Validation of a method for assay of sulfur hexafluoride in a new contrast agent by gas chromatography. Pharmaceutical Chemistry Journal, 51(3), 222-225. https://doi.org/10.1007/s11094-017-1586-3

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AU - Drygunova, L. A.

AU - Gur’ev, A. M.

AU - Belousov, M. V.

AU - Yusubov, M. S.

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Access to Document

10.1007/s11094-017-1586-3