Abstract
In this paper, the powders of brushite from an aqueous solution of Ca(NO3)2- (NH4)2HPO4 with different content of chitosan were synthesized. XRD data revealed that all samples are single-phase and are brushite (CaHPO4•2H2O). By FT-IR spectroscopy and BET methods, it was found that chitosan adsorbs onto the surface of powders. With increase of the content of the additive, the average size of crystallites increases 4.0 - 4.8 - 11.8 μm, respectively, and the dissolution rate in isotonic solution also decreases. The thermal stability of the composite powders was studied. It was established that the highest destruction of samples occurs in the range 473-673 K by removing of adsorption and crystallization water and partial change of the structure of the mineral and chitosan. At a temperature of 873 K, carbonization of the organic additive occurs.
| Original language | English |
|---|---|
| Article number | 012066 |
| Journal | IOP Conference Series: Materials Science and Engineering |
| Volume | 168 |
| Issue number | 1 |
| DOIs | |
| Publication status | Published - 7 Feb 2017 |
| Event | 12th International Conference Radiation-Thermal Effects and Processes in Inorganic Materials - Tomsk, Russian Federation Duration: 4 Sep 2016 → 12 Sep 2016 |
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ASJC Scopus subject areas
- Materials Science(all)
- Engineering(all)
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Thermal stability of brushite with chitosan samples. / Chikanova, E. S.; Golovanova, O. A.; Malikova, T. V.; Kuimova, M. V.
In: IOP Conference Series: Materials Science and Engineering, Vol. 168, No. 1, 012066, 07.02.2017.Research output: Contribution to journal › Article
}
TY - JOUR
T1 - Thermal stability of brushite with chitosan samples
AU - Chikanova, E. S.
AU - Golovanova, O. A.
AU - Malikova, T. V.
AU - Kuimova, M. V.
PY - 2017/2/7
Y1 - 2017/2/7
N2 - In this paper, the powders of brushite from an aqueous solution of Ca(NO3)2- (NH4)2HPO4 with different content of chitosan were synthesized. XRD data revealed that all samples are single-phase and are brushite (CaHPO4•2H2O). By FT-IR spectroscopy and BET methods, it was found that chitosan adsorbs onto the surface of powders. With increase of the content of the additive, the average size of crystallites increases 4.0 - 4.8 - 11.8 μm, respectively, and the dissolution rate in isotonic solution also decreases. The thermal stability of the composite powders was studied. It was established that the highest destruction of samples occurs in the range 473-673 K by removing of adsorption and crystallization water and partial change of the structure of the mineral and chitosan. At a temperature of 873 K, carbonization of the organic additive occurs.
AB - In this paper, the powders of brushite from an aqueous solution of Ca(NO3)2- (NH4)2HPO4 with different content of chitosan were synthesized. XRD data revealed that all samples are single-phase and are brushite (CaHPO4•2H2O). By FT-IR spectroscopy and BET methods, it was found that chitosan adsorbs onto the surface of powders. With increase of the content of the additive, the average size of crystallites increases 4.0 - 4.8 - 11.8 μm, respectively, and the dissolution rate in isotonic solution also decreases. The thermal stability of the composite powders was studied. It was established that the highest destruction of samples occurs in the range 473-673 K by removing of adsorption and crystallization water and partial change of the structure of the mineral and chitosan. At a temperature of 873 K, carbonization of the organic additive occurs.
UR - http://www.scopus.com/inward/record.url?scp=85014442313&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=85014442313&partnerID=8YFLogxK
U2 - 10.1088/1757-899X/168/1/012066
DO - 10.1088/1757-899X/168/1/012066
M3 - Article
VL - 168
JO - IOP Conference Series: Materials Science and Engineering
JF - IOP Conference Series: Materials Science and Engineering
SN - 1757-8981
IS - 1
M1 - 012066
ER -