The formation of stable hydrogen impermeable TiN-based coatings on zirconium alloy Zr1%Nb

Abstract

TiN coatings were deposited by DC reactive magnetron sputtering (dcMS) method on Zr1%Nb substrates with different film thickness. The influence of crystalline structure and thickness of the coatings on hydrogen permeation was investigated. The results revealed that the increase in thickness of the film reduced hydrogen permeability. 1.54 μm TiN deposited in N<inf>2</inf>/Ar gas mixture with a ratio of 3/1 reduces hydrogen permeation in more than two orders of magnitude at 350 °C. Adhesion strength decreased with increasing film thickness (0.55 to 2.04 μm) from 7.92 to 6.65 N, respectively. The Ti underlayer applied by arc ion plating (AIP) leads to the formation of stable Ti/TiN coatings on Zr1%Nb under thermocycling conditions up to 800 °C. Meanwhile, hydrogen permeation rate of Ti/TiN deposited by combination of AIP and dcMS remains at the same level with TiN deposited by dcMS.

Original language	English
Title of host publication	IOP Conference Series: Materials Science and Engineering
Publisher	Institute of Physics Publishing
Volume	81
Edition	1
DOIs	https://doi.org/10.1088/1757-899X/81/1/012017
Publication status	Published - 23 Apr 2015
Event	International Scientific Conference on Radiation-Thermal Effects and Processes in Inorganic Materials, RTEP 2014 - Tomsk, Russian Federation Duration: 3 Nov 2014 → 8 Nov 2014

Other

Other	International Scientific Conference on Radiation-Thermal Effects and Processes in Inorganic Materials, RTEP 2014
Country	Russian Federation
City	Tomsk
Period	3.11.14 → 8.11.14

ASJC Scopus subject areas

Engineering(all)
Materials Science(all)

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10.1088/1757-899X/81/1/012017

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Kashkarov, E. B., Nikitenkov, N. N., Tyurin, Y. I., Syrtanov, M. S., & Le, Z. (2015). The formation of stable hydrogen impermeable TiN-based coatings on zirconium alloy Zr1%Nb. In IOP Conference Series: Materials Science and Engineering (1 ed., Vol. 81). [012017] Institute of Physics Publishing. https://doi.org/10.1088/1757-899X/81/1/012017

The formation of stable hydrogen impermeable TiN-based coatings on zirconium alloy Zr1%Nb. / Kashkarov, Egor Borisovich ; Nikitenkov, N. N.; Tyurin, Yu I.; Syrtanov, Maxim Sergeevich; Le, Zhang.

IOP Conference Series: Materials Science and Engineering. Vol. 81 1. ed. Institute of Physics Publishing, 2015. 012017.

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Kashkarov, EB , Nikitenkov, NN , Tyurin, YI , Syrtanov, MS & Le, Z 2015, The formation of stable hydrogen impermeable TiN-based coatings on zirconium alloy Zr1%Nb. in IOP Conference Series: Materials Science and Engineering. 1 edn, vol. 81, 012017, Institute of Physics Publishing, International Scientific Conference on Radiation-Thermal Effects and Processes in Inorganic Materials, RTEP 2014, Tomsk, Russian Federation, 3.11.14. https://doi.org/10.1088/1757-899X/81/1/012017

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title = "The formation of stable hydrogen impermeable TiN-based coatings on zirconium alloy Zr1%Nb",

abstract = "TiN coatings were deposited by DC reactive magnetron sputtering (dcMS) method on Zr1%Nb substrates with different film thickness. The influence of crystalline structure and thickness of the coatings on hydrogen permeation was investigated. The results revealed that the increase in thickness of the film reduced hydrogen permeability. 1.54 μm TiN deposited in N2/Ar gas mixture with a ratio of 3/1 reduces hydrogen permeation in more than two orders of magnitude at 350 °C. Adhesion strength decreased with increasing film thickness (0.55 to 2.04 μm) from 7.92 to 6.65 N, respectively. The Ti underlayer applied by arc ion plating (AIP) leads to the formation of stable Ti/TiN coatings on Zr1%Nb under thermocycling conditions up to 800 °C. Meanwhile, hydrogen permeation rate of Ti/TiN deposited by combination of AIP and dcMS remains at the same level with TiN deposited by dcMS.",

author = "Kashkarov, {Egor Borisovich} and Nikitenkov, {N. N.} and Tyurin, {Yu I.} and Syrtanov, {Maxim Sergeevich} and Zhang Le",

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AU - Kashkarov, Egor Borisovich

AU - Nikitenkov, N. N.

AU - Tyurin, Yu I.

AU - Syrtanov, Maxim Sergeevich

AU - Le, Zhang

PY - 2015/4/23

Y1 - 2015/4/23

N2 - TiN coatings were deposited by DC reactive magnetron sputtering (dcMS) method on Zr1%Nb substrates with different film thickness. The influence of crystalline structure and thickness of the coatings on hydrogen permeation was investigated. The results revealed that the increase in thickness of the film reduced hydrogen permeability. 1.54 μm TiN deposited in N2/Ar gas mixture with a ratio of 3/1 reduces hydrogen permeation in more than two orders of magnitude at 350 °C. Adhesion strength decreased with increasing film thickness (0.55 to 2.04 μm) from 7.92 to 6.65 N, respectively. The Ti underlayer applied by arc ion plating (AIP) leads to the formation of stable Ti/TiN coatings on Zr1%Nb under thermocycling conditions up to 800 °C. Meanwhile, hydrogen permeation rate of Ti/TiN deposited by combination of AIP and dcMS remains at the same level with TiN deposited by dcMS.

AB - TiN coatings were deposited by DC reactive magnetron sputtering (dcMS) method on Zr1%Nb substrates with different film thickness. The influence of crystalline structure and thickness of the coatings on hydrogen permeation was investigated. The results revealed that the increase in thickness of the film reduced hydrogen permeability. 1.54 μm TiN deposited in N2/Ar gas mixture with a ratio of 3/1 reduces hydrogen permeation in more than two orders of magnitude at 350 °C. Adhesion strength decreased with increasing film thickness (0.55 to 2.04 μm) from 7.92 to 6.65 N, respectively. The Ti underlayer applied by arc ion plating (AIP) leads to the formation of stable Ti/TiN coatings on Zr1%Nb under thermocycling conditions up to 800 °C. Meanwhile, hydrogen permeation rate of Ti/TiN deposited by combination of AIP and dcMS remains at the same level with TiN deposited by dcMS.

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