Abstract
TiN coatings were deposited by DC reactive magnetron sputtering (dcMS) method on Zr1%Nb substrates with different film thickness. The influence of crystalline structure and thickness of the coatings on hydrogen permeation was investigated. The results revealed that the increase in thickness of the film reduced hydrogen permeability. 1.54 μm TiN deposited in N<inf>2</inf>/Ar gas mixture with a ratio of 3/1 reduces hydrogen permeation in more than two orders of magnitude at 350 °C. Adhesion strength decreased with increasing film thickness (0.55 to 2.04 μm) from 7.92 to 6.65 N, respectively. The Ti underlayer applied by arc ion plating (AIP) leads to the formation of stable Ti/TiN coatings on Zr1%Nb under thermocycling conditions up to 800 °C. Meanwhile, hydrogen permeation rate of Ti/TiN deposited by combination of AIP and dcMS remains at the same level with TiN deposited by dcMS.
| Original language | English |
|---|---|
| Title of host publication | IOP Conference Series: Materials Science and Engineering |
| Publisher | Institute of Physics Publishing |
| Volume | 81 |
| Edition | 1 |
| DOIs | |
| Publication status | Published - 23 Apr 2015 |
| Event | International Scientific Conference on Radiation-Thermal Effects and Processes in Inorganic Materials, RTEP 2014 - Tomsk, Russian Federation Duration: 3 Nov 2014 → 8 Nov 2014 |
Other
| Other | International Scientific Conference on Radiation-Thermal Effects and Processes in Inorganic Materials, RTEP 2014 |
|---|---|
| Country | Russian Federation |
| City | Tomsk |
| Period | 3.11.14 → 8.11.14 |
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ASJC Scopus subject areas
- Engineering(all)
- Materials Science(all)
Cite this
The formation of stable hydrogen impermeable TiN-based coatings on zirconium alloy Zr1%Nb. / Kashkarov, Egor Borisovich; Nikitenkov, N. N.; Tyurin, Yu I.; Syrtanov, Maxim Sergeevich; Le, Zhang.
IOP Conference Series: Materials Science and Engineering. Vol. 81 1. ed. Institute of Physics Publishing, 2015. 012017.Research output: Chapter in Book/Report/Conference proceeding › Conference contribution
}
TY - GEN
T1 - The formation of stable hydrogen impermeable TiN-based coatings on zirconium alloy Zr1%Nb
AU - Kashkarov, Egor Borisovich
AU - Nikitenkov, N. N.
AU - Tyurin, Yu I.
AU - Syrtanov, Maxim Sergeevich
AU - Le, Zhang
PY - 2015/4/23
Y1 - 2015/4/23
N2 - TiN coatings were deposited by DC reactive magnetron sputtering (dcMS) method on Zr1%Nb substrates with different film thickness. The influence of crystalline structure and thickness of the coatings on hydrogen permeation was investigated. The results revealed that the increase in thickness of the film reduced hydrogen permeability. 1.54 μm TiN deposited in N2/Ar gas mixture with a ratio of 3/1 reduces hydrogen permeation in more than two orders of magnitude at 350 °C. Adhesion strength decreased with increasing film thickness (0.55 to 2.04 μm) from 7.92 to 6.65 N, respectively. The Ti underlayer applied by arc ion plating (AIP) leads to the formation of stable Ti/TiN coatings on Zr1%Nb under thermocycling conditions up to 800 °C. Meanwhile, hydrogen permeation rate of Ti/TiN deposited by combination of AIP and dcMS remains at the same level with TiN deposited by dcMS.
AB - TiN coatings were deposited by DC reactive magnetron sputtering (dcMS) method on Zr1%Nb substrates with different film thickness. The influence of crystalline structure and thickness of the coatings on hydrogen permeation was investigated. The results revealed that the increase in thickness of the film reduced hydrogen permeability. 1.54 μm TiN deposited in N2/Ar gas mixture with a ratio of 3/1 reduces hydrogen permeation in more than two orders of magnitude at 350 °C. Adhesion strength decreased with increasing film thickness (0.55 to 2.04 μm) from 7.92 to 6.65 N, respectively. The Ti underlayer applied by arc ion plating (AIP) leads to the formation of stable Ti/TiN coatings on Zr1%Nb under thermocycling conditions up to 800 °C. Meanwhile, hydrogen permeation rate of Ti/TiN deposited by combination of AIP and dcMS remains at the same level with TiN deposited by dcMS.
UR - http://www.scopus.com/inward/record.url?scp=84930428246&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=84930428246&partnerID=8YFLogxK
U2 - 10.1088/1757-899X/81/1/012017
DO - 10.1088/1757-899X/81/1/012017
M3 - Conference contribution
VL - 81
BT - IOP Conference Series: Materials Science and Engineering
PB - Institute of Physics Publishing
ER -