Synthesis of ultra dispersed graphite-like structures doped with nitrogen in supersonic carbon plasma flow

Research output: Chapter in Book/Report/Conference proceedingConference contribution

3 Citations (Scopus)

Abstract

In this paper the synthesis of ultra dispersed graphite-like structures doped with nitrogen by using a magneto plasma accelerator is shown. The synthesis of such structures is realized during supersonic carbon plasma jet flowing into the chamber filled with the nitrogen atmosphere. Plasma jet is generated by coaxial magneto plasma accelerator (CMPA) based on graphite electrode system. The CMPA is supplied from the pulsed capacitive energy storage with the maximum value of stored energy of 360 kJ. Electrical and energy parameters of plasma flow are recorded during experiment. According to X-ray diffraction (XRD) and high resolution transmission electron microscopy (HRTEM) methods obtained particles with well seen triangle sectors are graphite-like carbon structures doped with nitrogen atoms. This is confirmed by X-ray photoelectron spectroscopy (XPS) and Raman spectroscopy analyses in which carbon- nitrogen bonding configurations have been identified.

Original languageEnglish
Title of host publicationIOP Conference Series: Materials Science and Engineering
PublisherInstitute of Physics Publishing
Volume66
Edition1
DOIs
Publication statusPublished - 2014
Event20th International Conference for Students and Young Scientists: Modern Techniques and Technologies, MTT 2014 - Tomsk, Russian Federation
Duration: 14 Apr 201418 Apr 2014

Other

Other20th International Conference for Students and Young Scientists: Modern Techniques and Technologies, MTT 2014
CountryRussian Federation
CityTomsk
Period14.4.1418.4.14

Fingerprint

Plasma flow
Graphite
Plasma accelerators
Nitrogen
Carbon
Plasma jets
Graphite electrodes
High resolution transmission electron microscopy
Energy storage
Raman spectroscopy
X ray photoelectron spectroscopy
X ray diffraction
Atoms
Experiments

ASJC Scopus subject areas

  • Engineering(all)
  • Materials Science(all)

Cite this

Sivkov, A., Pak, A., Shanenkov, I., Kolganova, J., & Shatrova, K. (2014). Synthesis of ultra dispersed graphite-like structures doped with nitrogen in supersonic carbon plasma flow. In IOP Conference Series: Materials Science and Engineering (1 ed., Vol. 66). [012001] Institute of Physics Publishing. https://doi.org/10.1088/1757-899X/66/1/012001

Synthesis of ultra dispersed graphite-like structures doped with nitrogen in supersonic carbon plasma flow. / Sivkov, A.; Pak, A.; Shanenkov, I.; Kolganova, J.; Shatrova, K.

IOP Conference Series: Materials Science and Engineering. Vol. 66 1. ed. Institute of Physics Publishing, 2014. 012001.

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Sivkov, A, Pak, A, Shanenkov, I, Kolganova, J & Shatrova, K 2014, Synthesis of ultra dispersed graphite-like structures doped with nitrogen in supersonic carbon plasma flow. in IOP Conference Series: Materials Science and Engineering. 1 edn, vol. 66, 012001, Institute of Physics Publishing, 20th International Conference for Students and Young Scientists: Modern Techniques and Technologies, MTT 2014, Tomsk, Russian Federation, 14.4.14. https://doi.org/10.1088/1757-899X/66/1/012001
Sivkov A, Pak A, Shanenkov I, Kolganova J, Shatrova K. Synthesis of ultra dispersed graphite-like structures doped with nitrogen in supersonic carbon plasma flow. In IOP Conference Series: Materials Science and Engineering. 1 ed. Vol. 66. Institute of Physics Publishing. 2014. 012001 https://doi.org/10.1088/1757-899X/66/1/012001
Sivkov, A. ; Pak, A. ; Shanenkov, I. ; Kolganova, J. ; Shatrova, K. / Synthesis of ultra dispersed graphite-like structures doped with nitrogen in supersonic carbon plasma flow. IOP Conference Series: Materials Science and Engineering. Vol. 66 1. ed. Institute of Physics Publishing, 2014.
@inproceedings{ea95cdf3fd8648f493586632826e8057,
title = "Synthesis of ultra dispersed graphite-like structures doped with nitrogen in supersonic carbon plasma flow",
abstract = "In this paper the synthesis of ultra dispersed graphite-like structures doped with nitrogen by using a magneto plasma accelerator is shown. The synthesis of such structures is realized during supersonic carbon plasma jet flowing into the chamber filled with the nitrogen atmosphere. Plasma jet is generated by coaxial magneto plasma accelerator (CMPA) based on graphite electrode system. The CMPA is supplied from the pulsed capacitive energy storage with the maximum value of stored energy of 360 kJ. Electrical and energy parameters of plasma flow are recorded during experiment. According to X-ray diffraction (XRD) and high resolution transmission electron microscopy (HRTEM) methods obtained particles with well seen triangle sectors are graphite-like carbon structures doped with nitrogen atoms. This is confirmed by X-ray photoelectron spectroscopy (XPS) and Raman spectroscopy analyses in which carbon- nitrogen bonding configurations have been identified.",
author = "A. Sivkov and A. Pak and I. Shanenkov and J. Kolganova and K. Shatrova",
year = "2014",
doi = "10.1088/1757-899X/66/1/012001",
language = "English",
volume = "66",
booktitle = "IOP Conference Series: Materials Science and Engineering",
publisher = "Institute of Physics Publishing",
edition = "1",

}

TY - GEN

T1 - Synthesis of ultra dispersed graphite-like structures doped with nitrogen in supersonic carbon plasma flow

AU - Sivkov, A.

AU - Pak, A.

AU - Shanenkov, I.

AU - Kolganova, J.

AU - Shatrova, K.

PY - 2014

Y1 - 2014

N2 - In this paper the synthesis of ultra dispersed graphite-like structures doped with nitrogen by using a magneto plasma accelerator is shown. The synthesis of such structures is realized during supersonic carbon plasma jet flowing into the chamber filled with the nitrogen atmosphere. Plasma jet is generated by coaxial magneto plasma accelerator (CMPA) based on graphite electrode system. The CMPA is supplied from the pulsed capacitive energy storage with the maximum value of stored energy of 360 kJ. Electrical and energy parameters of plasma flow are recorded during experiment. According to X-ray diffraction (XRD) and high resolution transmission electron microscopy (HRTEM) methods obtained particles with well seen triangle sectors are graphite-like carbon structures doped with nitrogen atoms. This is confirmed by X-ray photoelectron spectroscopy (XPS) and Raman spectroscopy analyses in which carbon- nitrogen bonding configurations have been identified.

AB - In this paper the synthesis of ultra dispersed graphite-like structures doped with nitrogen by using a magneto plasma accelerator is shown. The synthesis of such structures is realized during supersonic carbon plasma jet flowing into the chamber filled with the nitrogen atmosphere. Plasma jet is generated by coaxial magneto plasma accelerator (CMPA) based on graphite electrode system. The CMPA is supplied from the pulsed capacitive energy storage with the maximum value of stored energy of 360 kJ. Electrical and energy parameters of plasma flow are recorded during experiment. According to X-ray diffraction (XRD) and high resolution transmission electron microscopy (HRTEM) methods obtained particles with well seen triangle sectors are graphite-like carbon structures doped with nitrogen atoms. This is confirmed by X-ray photoelectron spectroscopy (XPS) and Raman spectroscopy analyses in which carbon- nitrogen bonding configurations have been identified.

UR - http://www.scopus.com/inward/record.url?scp=84907782113&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=84907782113&partnerID=8YFLogxK

U2 - 10.1088/1757-899X/66/1/012001

DO - 10.1088/1757-899X/66/1/012001

M3 - Conference contribution

VL - 66

BT - IOP Conference Series: Materials Science and Engineering

PB - Institute of Physics Publishing

ER -