Synthesis of Ti3SiC2-based composites by spark plasma sintering of preceramic papers

Research output: Contribution to journalConference article

Abstract

This paper is devoted to fabrication of Ti3SiC2-based ceramic materials from preceramic paper using spark plasma sintering (SPS) method. The synthesis temperature and pressure were 1373-1473 K and 30 MPa, respectively. The phase composition, microstructure and elemental composition were analysed using X-ray diffraction, scanning electron microscopy and energy-dispersive X-ray spectroscopy, respectively. The effect of temperature on the sintering process as well as on the phase and microstructure of the sintered materials was investigated.

Original languageEnglish
Article number012058
JournalIOP Conference Series: Materials Science and Engineering
Volume597
Issue number1
DOIs
Publication statusPublished - 23 Aug 2019
Event16th International Conference of Students and Young Scientists on Prospects of Fundamental Sciences Development, PFSD 2019 - Tomsk, Russian Federation
Duration: 23 Apr 201926 Apr 2019

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Spark plasma sintering
Microstructure
Composite materials
Ceramic materials
Phase composition
Sintering
Fabrication
X ray diffraction
Temperature
Scanning electron microscopy
Chemical analysis
Ti3SiC2
X-Ray Emission Spectrometry

ASJC Scopus subject areas

  • Materials Science(all)
  • Engineering(all)

Cite this

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title = "Synthesis of Ti3SiC2-based composites by spark plasma sintering of preceramic papers",
abstract = "This paper is devoted to fabrication of Ti3SiC2-based ceramic materials from preceramic paper using spark plasma sintering (SPS) method. The synthesis temperature and pressure were 1373-1473 K and 30 MPa, respectively. The phase composition, microstructure and elemental composition were analysed using X-ray diffraction, scanning electron microscopy and energy-dispersive X-ray spectroscopy, respectively. The effect of temperature on the sintering process as well as on the phase and microstructure of the sintered materials was investigated.",
author = "Kashkarov, {E. B.} and Syrtanov, {M. S.} and Sedanova, {E. P.} and Ivashutenko, {A. S.} and Lider, {A. M.} and N. Travitzky",
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AU - Kashkarov, E. B.

AU - Syrtanov, M. S.

AU - Sedanova, E. P.

AU - Ivashutenko, A. S.

AU - Lider, A. M.

AU - Travitzky, N.

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AB - This paper is devoted to fabrication of Ti3SiC2-based ceramic materials from preceramic paper using spark plasma sintering (SPS) method. The synthesis temperature and pressure were 1373-1473 K and 30 MPa, respectively. The phase composition, microstructure and elemental composition were analysed using X-ray diffraction, scanning electron microscopy and energy-dispersive X-ray spectroscopy, respectively. The effect of temperature on the sintering process as well as on the phase and microstructure of the sintered materials was investigated.

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