Synthesis of substituted lithium ferrites under the pulsed and continuous electron beam heating

Abstract

Synthesis of substituted lithium ferrites with chemical formulas Li_0.6Fe_2.2Ti_0.2O₄ and Li_0.649Fe_1.598Ti_0.5Zn_0.2Mn_0.051O₄ under the pulsed and continuous electron beam heating was investigated by X-ray diffraction and thermomagnetometric analysis. The electron beams heating of Li₂CO₃-Fe₂O₃-TiO₂ or Li₂CO₃-ZnO-Fe₂O₃-TiO₂-MnO mixtures was carried out at a temperature of 750 °C during 60 min using two types of electron accelerators: ELV accelerator generating continuous electron beam or ILU-6 accelerator generating pulse electron beam. It was established that a high energy electron beam heating of initial reagents mixtures allows obtaining the substituted lithium ferrites with final composition at significantly lower temperatures (at least 200 °C lower than in the case of using traditional thermal synthesis) and times of synthesis. That statement is in agreement with results obtained by XRD analysis, showing single phase formation; by magnetic measurements, showing high values of specific magnetization; by DTG measurements showing the certain Curie temperatures of the synthesized samples.

Original language	English
Pages (from-to)	1-7
Number of pages	7
Journal	Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms
Volume	392
DOIs	https://doi.org/10.1016/j.nimb.2016.11.042
Publication status	Published - 1 Feb 2017

Keywords

Electron beam
Radiation-thermal heating
Substituted lithium ferrites
Synthesis

ASJC Scopus subject areas

Nuclear and High Energy Physics
Instrumentation

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10.1016/j.nimb.2016.11.042

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Lysenko, E. N., Surzhikov, A. P., Vlasov, V. A., Nikolaev, E. V., Malyshev, A. V., Bryazgin, A. A., Korobeynikov, M. V., & Mikhailenko, M. A. (2017). Synthesis of substituted lithium ferrites under the pulsed and continuous electron beam heating. Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms, 392, 1-7. https://doi.org/10.1016/j.nimb.2016.11.042

Synthesis of substituted lithium ferrites under the pulsed and continuous electron beam heating. / Lysenko, Elena N.; Surzhikov, Anatoliy P.; Vlasov, Vitaliy A.; Nikolaev, Evgeniy V.; Malyshev, Andrey V.; Bryazgin, Alexandr A.; Korobeynikov, Mikhail V.; Mikhailenko, Mikhail A.

In: Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms, Vol. 392, 01.02.2017, p. 1-7.

Research output: Contribution to journal › Article › peer-review

Lysenko, EN , Surzhikov, AP , Vlasov, VA , Nikolaev, EV , Malyshev, AV, Bryazgin, AA, Korobeynikov, MV & Mikhailenko, MA 2017, 'Synthesis of substituted lithium ferrites under the pulsed and continuous electron beam heating', Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms, vol. 392, pp. 1-7. https://doi.org/10.1016/j.nimb.2016.11.042

Lysenko, Elena N. ; Surzhikov, Anatoliy P. ; Vlasov, Vitaliy A. ; Nikolaev, Evgeniy V. ; Malyshev, Andrey V. ; Bryazgin, Alexandr A. ; Korobeynikov, Mikhail V. ; Mikhailenko, Mikhail A. / Synthesis of substituted lithium ferrites under the pulsed and continuous electron beam heating. In: Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms. 2017 ; Vol. 392. pp. 1-7.

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title = "Synthesis of substituted lithium ferrites under the pulsed and continuous electron beam heating",

abstract = "Synthesis of substituted lithium ferrites with chemical formulas Li0.6Fe2.2Ti0.2O4 and Li0.649Fe1.598Ti0.5Zn0.2Mn0.051O4 under the pulsed and continuous electron beam heating was investigated by X-ray diffraction and thermomagnetometric analysis. The electron beams heating of Li2CO3-Fe2O3-TiO2 or Li2CO3-ZnO-Fe2O3-TiO2-MnO mixtures was carried out at a temperature of 750 °C during 60 min using two types of electron accelerators: ELV accelerator generating continuous electron beam or ILU-6 accelerator generating pulse electron beam. It was established that a high energy electron beam heating of initial reagents mixtures allows obtaining the substituted lithium ferrites with final composition at significantly lower temperatures (at least 200 °C lower than in the case of using traditional thermal synthesis) and times of synthesis. That statement is in agreement with results obtained by XRD analysis, showing single phase formation; by magnetic measurements, showing high values of specific magnetization; by DTG measurements showing the certain Curie temperatures of the synthesized samples.",

keywords = "Electron beam, Radiation-thermal heating, Substituted lithium ferrites, Synthesis",

author = "Lysenko, {Elena N.} and Surzhikov, {Anatoliy P.} and Vlasov, {Vitaliy A.} and Nikolaev, {Evgeniy V.} and Malyshev, {Andrey V.} and Bryazgin, {Alexandr A.} and Korobeynikov, {Mikhail V.} and Mikhailenko, {Mikhail A.}",

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AU - Surzhikov, Anatoliy P.

AU - Vlasov, Vitaliy A.

AU - Nikolaev, Evgeniy V.

AU - Malyshev, Andrey V.

AU - Bryazgin, Alexandr A.

AU - Korobeynikov, Mikhail V.

AU - Mikhailenko, Mikhail A.

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N2 - Synthesis of substituted lithium ferrites with chemical formulas Li0.6Fe2.2Ti0.2O4 and Li0.649Fe1.598Ti0.5Zn0.2Mn0.051O4 under the pulsed and continuous electron beam heating was investigated by X-ray diffraction and thermomagnetometric analysis. The electron beams heating of Li2CO3-Fe2O3-TiO2 or Li2CO3-ZnO-Fe2O3-TiO2-MnO mixtures was carried out at a temperature of 750 °C during 60 min using two types of electron accelerators: ELV accelerator generating continuous electron beam or ILU-6 accelerator generating pulse electron beam. It was established that a high energy electron beam heating of initial reagents mixtures allows obtaining the substituted lithium ferrites with final composition at significantly lower temperatures (at least 200 °C lower than in the case of using traditional thermal synthesis) and times of synthesis. That statement is in agreement with results obtained by XRD analysis, showing single phase formation; by magnetic measurements, showing high values of specific magnetization; by DTG measurements showing the certain Curie temperatures of the synthesized samples.

AB - Synthesis of substituted lithium ferrites with chemical formulas Li0.6Fe2.2Ti0.2O4 and Li0.649Fe1.598Ti0.5Zn0.2Mn0.051O4 under the pulsed and continuous electron beam heating was investigated by X-ray diffraction and thermomagnetometric analysis. The electron beams heating of Li2CO3-Fe2O3-TiO2 or Li2CO3-ZnO-Fe2O3-TiO2-MnO mixtures was carried out at a temperature of 750 °C during 60 min using two types of electron accelerators: ELV accelerator generating continuous electron beam or ILU-6 accelerator generating pulse electron beam. It was established that a high energy electron beam heating of initial reagents mixtures allows obtaining the substituted lithium ferrites with final composition at significantly lower temperatures (at least 200 °C lower than in the case of using traditional thermal synthesis) and times of synthesis. That statement is in agreement with results obtained by XRD analysis, showing single phase formation; by magnetic measurements, showing high values of specific magnetization; by DTG measurements showing the certain Curie temperatures of the synthesized samples.

KW - Electron beam

KW - Radiation-thermal heating

KW - Substituted lithium ferrites

KW - Synthesis

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