Synthesis and properties of lead nanoparticles

Dmitry Vasilievich Akimov, O. S. Andrienko, N. B. Egorov, I. I. Zherin, V. F. Usov

Research output: Contribution to journalArticle

2 Citations (Scopus)

Abstract

Lead nanoparticles were synthesized by the thermal decomposition of lead stearate in octanol. The nanoparticles were characterized by X-ray powder diffraction, thermal analysis, IR spectroscopy, and electron microscopy. The lead particle size can be controlled by both varying the concentration of lead stearate in octanol and changing the thermolysis time. Lead nanoparticles have an organic coat composed of decomposition products of lead stearate. This coat prevents the particles from oxidation in air and favors their dissolution in organic solvents.

Original languageEnglish
Pages (from-to)225-229
Number of pages5
JournalRussian Chemical Bulletin
Volume61
Issue number2
DOIs
Publication statusPublished - 1 Feb 2012

Fingerprint

Stearates
Nanoparticles
Octanols
Thermolysis
X ray powder diffraction
Organic solvents
Thermoanalysis
Electron microscopy
Infrared spectroscopy
Dissolution
Pyrolysis
Particle size
Lead
Decomposition
Oxidation
Air

Keywords

  • lead
  • lead stearate
  • nanoparticles
  • synthesis
  • thermolysis

ASJC Scopus subject areas

  • Chemistry(all)

Cite this

Synthesis and properties of lead nanoparticles. / Akimov, Dmitry Vasilievich; Andrienko, O. S.; Egorov, N. B.; Zherin, I. I.; Usov, V. F.

In: Russian Chemical Bulletin, Vol. 61, No. 2, 01.02.2012, p. 225-229.

Research output: Contribution to journalArticle

Akimov, Dmitry Vasilievich ; Andrienko, O. S. ; Egorov, N. B. ; Zherin, I. I. ; Usov, V. F. / Synthesis and properties of lead nanoparticles. In: Russian Chemical Bulletin. 2012 ; Vol. 61, No. 2. pp. 225-229.
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