Synthesis and characterization of LiClO4 center dot H2O

S. I. Ivlev, Dmitry Vasilievich Akimov, N. B. Egorov, F. Kraus

Research output: Contribution to journalArticle

1 Citation (Scopus)

Abstract

Lithium perchlorate monohydrate was synthesized and characterized. The compound crystallizes isotypic to sodium perchlorate monohydrate in the monoclinic space group type C2/c with a = 14.2592(6) Å, b = 5.2921(2) Å, c = 10.3382(4) Å, β = 111.765(2)°, V = 724.52(5) Å3, Z = 8, at T = 110 K. Additionally, we investigated the compound by means of IR and Raman spectroscopy, powder X-ray diffraction, thermal analysis (TG/DSC), and solid-state computational calculations.

Original languageEnglish
Pages (from-to)279-288
Number of pages10
JournalMonatshefte fur Chemie
Volume147
Issue number2
DOIs
Publication statusPublished - Feb 2016

Keywords

  • DFT calculations
  • IR spectra
  • Lithium
  • Perchlorate
  • Raman spectra
  • Single crystal diffraction

ASJC Scopus subject areas

  • Chemistry(all)

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