Synthesis and characterization of LiClO4 center dot H2O

S. I. Ivlev, Dmitry Vasilievich Akimov, N. B. Egorov, F. Kraus

Research output: Contribution to journalArticle

1 Citation (Scopus)

Abstract

Lithium perchlorate monohydrate was synthesized and characterized. The compound crystallizes isotypic to sodium perchlorate monohydrate in the monoclinic space group type C2/c with a = 14.2592(6) Å, b = 5.2921(2) Å, c = 10.3382(4) Å, β = 111.765(2)°, V = 724.52(5) Å3, Z = 8, at T = 110 K. Additionally, we investigated the compound by means of IR and Raman spectroscopy, powder X-ray diffraction, thermal analysis (TG/DSC), and solid-state computational calculations.

Original languageEnglish
Pages (from-to)279-288
Number of pages10
JournalMonatshefte fur Chemie
Volume147
Issue number2
DOIs
Publication statusPublished - Feb 2016

Fingerprint

X ray powder diffraction
Thermoanalysis
Raman spectroscopy
Infrared spectroscopy
sodium perchlorate
lithium perchlorate

Keywords

  • DFT calculations
  • IR spectra
  • Lithium
  • Perchlorate
  • Raman spectra
  • Single crystal diffraction

ASJC Scopus subject areas

  • Chemistry(all)

Cite this

Synthesis and characterization of LiClO4 center dot H2O. / Ivlev, S. I.; Akimov, Dmitry Vasilievich; Egorov, N. B.; Kraus, F.

In: Monatshefte fur Chemie, Vol. 147, No. 2, 02.2016, p. 279-288.

Research output: Contribution to journalArticle

Ivlev, S. I. ; Akimov, Dmitry Vasilievich ; Egorov, N. B. ; Kraus, F. / Synthesis and characterization of LiClO4 center dot H2O. In: Monatshefte fur Chemie. 2016 ; Vol. 147, No. 2. pp. 279-288.
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KW - Raman spectra

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