Structure of nanotubular titanium oxide templates prepared by electrochemical anodization in H2SO4/HF solutions

Abstract

The electrochemical formation of nanotubular titanium oxide films was investigated in 1 M H₂SO₄ and 0.05-0.4 wt.% HF electrolytes. Depending on anodization condition, i.e. cell voltage, anodization time, HF concentration, TiO₂ porous films having different thickness (from 350 to 500 nm) and pore diameter (from 40 to 150 nm) were obtained. By varying the cell voltage from 10 V to 40 V it was possible to gradually change the crystal structure of titanium oxide from anatase to rutile. The effect of annealing temperature and duration on crystal structure was also considered.

Original language	English
Pages (from-to)	5253-5258
Number of pages	6
Journal	Thin Solid Films
Volume	515
Issue number	13
DOIs	https://doi.org/10.1016/j.tsf.2006.12.180
Publication status	Published - 7 May 2007
Externally published	Yes

Keywords

Anatase
Nanostructures
Rutile
Templates
Titanium oxide

ASJC Scopus subject areas

Surfaces, Coatings and Films
Condensed Matter Physics
Surfaces and Interfaces

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10.1016/j.tsf.2006.12.180

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@article{0424265574334859805e0bd09566ad66,

title = "Structure of nanotubular titanium oxide templates prepared by electrochemical anodization in H2SO4/HF solutions",

abstract = "The electrochemical formation of nanotubular titanium oxide films was investigated in 1 M H2SO4 and 0.05-0.4 wt.% HF electrolytes. Depending on anodization condition, i.e. cell voltage, anodization time, HF concentration, TiO2 porous films having different thickness (from 350 to 500 nm) and pore diameter (from 40 to 150 nm) were obtained. By varying the cell voltage from 10 V to 40 V it was possible to gradually change the crystal structure of titanium oxide from anatase to rutile. The effect of annealing temperature and duration on crystal structure was also considered.",

keywords = "Anatase, Nanostructures, Rutile, Templates, Titanium oxide",

author = "M. Bestetti and S. Franz and M. Cuzzolin and P. Arosio and Cavallotti, {P. L.}",

year = "2007",

month = may,

day = "7",

doi = "10.1016/j.tsf.2006.12.180",

language = "English",

volume = "515",

pages = "5253--5258",

journal = "Thin Solid Films",

issn = "0040-6090",

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number = "13",

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T1 - Structure of nanotubular titanium oxide templates prepared by electrochemical anodization in H2SO4/HF solutions

AU - Bestetti, M.

AU - Franz, S.

AU - Cuzzolin, M.

AU - Arosio, P.

AU - Cavallotti, P. L.

PY - 2007/5/7

Y1 - 2007/5/7

N2 - The electrochemical formation of nanotubular titanium oxide films was investigated in 1 M H2SO4 and 0.05-0.4 wt.% HF electrolytes. Depending on anodization condition, i.e. cell voltage, anodization time, HF concentration, TiO2 porous films having different thickness (from 350 to 500 nm) and pore diameter (from 40 to 150 nm) were obtained. By varying the cell voltage from 10 V to 40 V it was possible to gradually change the crystal structure of titanium oxide from anatase to rutile. The effect of annealing temperature and duration on crystal structure was also considered.

AB - The electrochemical formation of nanotubular titanium oxide films was investigated in 1 M H2SO4 and 0.05-0.4 wt.% HF electrolytes. Depending on anodization condition, i.e. cell voltage, anodization time, HF concentration, TiO2 porous films having different thickness (from 350 to 500 nm) and pore diameter (from 40 to 150 nm) were obtained. By varying the cell voltage from 10 V to 40 V it was possible to gradually change the crystal structure of titanium oxide from anatase to rutile. The effect of annealing temperature and duration on crystal structure was also considered.

KW - Anatase

KW - Nanostructures

KW - Rutile

KW - Templates

KW - Titanium oxide

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U2 - 10.1016/j.tsf.2006.12.180

DO - 10.1016/j.tsf.2006.12.180

M3 - Article

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VL - 515

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EP - 5258

JO - Thin Solid Films

JF - Thin Solid Films

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