Sol-gel synthesis of chelate containing materials for gas chromatography

Abstract

The adsorption properties of mesoporous chelate containing sorbents which were prepared in two phases with europium and copper acetylacetonate complexes and PEG-115 as surfactant, were evaluated by column experiments. The adsorption properties of mesoporous silica with chelate complexes for some organic compounds were evaluated by gas chromatography. The best separation was achieved for europium acetylacetonate. From specific retention volumes measured at various temperatures the thermodynamic parameters of separation is discussed. Mutual separation of oxygen containing substances could also be demonstrated.

Original language	English
Title of host publication	Advanced Materials Research
Publisher	Trans Tech Publications Ltd
Pages	448-452
Number of pages	5
Volume	1040
ISBN (Print)	9783038352648
DOIs	https://doi.org/10.4028/www.scientific.net/AMR.1040.448
Publication status	Published - 2014
Event	International Conference for Young Scientists “High Technology: Research and Applications 2014”, HTRA 2014 - Tomsk, Russian Federation Duration: 26 Mar 2014 → 28 Mar 2014

Publication series

Name	Advanced Materials Research
Volume	1040
ISSN (Print)	10226680
ISSN (Electronic)	16628985

Other

Other	International Conference for Young Scientists “High Technology: Research and Applications 2014”, HTRA 2014
Country	Russian Federation
City	Tomsk
Period	26.3.14 → 28.3.14

Keywords

Chelate
Gas chromatography
Sorbent
Synthesis

ASJC Scopus subject areas

Engineering(all)

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10.4028/www.scientific.net/AMR.1040.448

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Cite this

Gavrilenko, M. A., Slizhov, Y. G., Faustova, Z. V., Kasymova, T. A., & Gavrilenko, N. A. (2014). Sol-gel synthesis of chelate containing materials for gas chromatography. In Advanced Materials Research (Vol. 1040, pp. 448-452). (Advanced Materials Research; Vol. 1040). Trans Tech Publications Ltd. https://doi.org/10.4028/www.scientific.net/AMR.1040.448

Sol-gel synthesis of chelate containing materials for gas chromatography. / Gavrilenko, Mikhail A.; Slizhov, Yurii G.; Faustova, Zhanna V.; Kasymova, Tatiana A.; Gavrilenko, Nataliya Airatovna.

Advanced Materials Research. Vol. 1040 Trans Tech Publications Ltd, 2014. p. 448-452 (Advanced Materials Research; Vol. 1040).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Gavrilenko, MA, Slizhov, YG, Faustova, ZV, Kasymova, TA & Gavrilenko, NA 2014, Sol-gel synthesis of chelate containing materials for gas chromatography. in Advanced Materials Research. vol. 1040, Advanced Materials Research, vol. 1040, Trans Tech Publications Ltd, pp. 448-452, International Conference for Young Scientists “High Technology: Research and Applications 2014”, HTRA 2014, Tomsk, Russian Federation, 26.3.14. https://doi.org/10.4028/www.scientific.net/AMR.1040.448

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title = "Sol-gel synthesis of chelate containing materials for gas chromatography",

abstract = "The adsorption properties of mesoporous chelate containing sorbents which were prepared in two phases with europium and copper acetylacetonate complexes and PEG-115 as surfactant, were evaluated by column experiments. The adsorption properties of mesoporous silica with chelate complexes for some organic compounds were evaluated by gas chromatography. The best separation was achieved for europium acetylacetonate. From specific retention volumes measured at various temperatures the thermodynamic parameters of separation is discussed. Mutual separation of oxygen containing substances could also be demonstrated.",

keywords = "Chelate, Gas chromatography, Sorbent, Synthesis",

author = "Gavrilenko, {Mikhail A.} and Slizhov, {Yurii G.} and Faustova, {Zhanna V.} and Kasymova, {Tatiana A.} and Gavrilenko, {Nataliya Airatovna}",

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AU - Gavrilenko, Mikhail A.

AU - Slizhov, Yurii G.

AU - Faustova, Zhanna V.

AU - Kasymova, Tatiana A.

AU - Gavrilenko, Nataliya Airatovna

PY - 2014

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AB - The adsorption properties of mesoporous chelate containing sorbents which were prepared in two phases with europium and copper acetylacetonate complexes and PEG-115 as surfactant, were evaluated by column experiments. The adsorption properties of mesoporous silica with chelate complexes for some organic compounds were evaluated by gas chromatography. The best separation was achieved for europium acetylacetonate. From specific retention volumes measured at various temperatures the thermodynamic parameters of separation is discussed. Mutual separation of oxygen containing substances could also be demonstrated.

KW - Chelate

KW - Gas chromatography

KW - Sorbent

KW - Synthesis

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PB - Trans Tech Publications Ltd

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