Sintering of zirconia ceramics by intense high-energy electron beam

Abstract

A comparative analysis of the efficiency of zirconia ceramics sintering by thermal method and high-energy electron beam sintering was performed for compacts prepared from commercial TZ-3Y-E grade powder. The electron energy was 1.4 MeV. The samples were sintered in the temperature range of 1200–1400 °C. Sintering of zirconia ceramics by high-energy accelerated electron beam is shown to reduce the firing temperature by about 200 °C compared to that in conventional heating technique. Ceramics sintered by accelerated electron beam at 1200 °C is of high density, microhardness and smaller grain size compared to that produced by thermal firing at 1400 °C. Electron beam sintering at higher temperature causes deterioration of ceramics properties due to radiation-induced acceleration of high-temperature recrystallization at higher temperatures.

Original language	English
Pages (from-to)	13888-13892
Number of pages	5
Journal	Ceramics International
Volume	42
Issue number	12
DOIs	https://doi.org/10.1016/j.ceramint.2016.05.198
Publication status	Published - 1 Sep 2016

Keywords

Grain size
Hardness
High-energy electron beam sintering
Zro

ASJC Scopus subject areas

Electronic, Optical and Magnetic Materials
Ceramics and Composites
Process Chemistry and Technology
Surfaces, Coatings and Films
Materials Chemistry

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@article{702bf3e697e941b18e0eafe4e58787f2,

title = "Sintering of zirconia ceramics by intense high-energy electron beam",

abstract = "A comparative analysis of the efficiency of zirconia ceramics sintering by thermal method and high-energy electron beam sintering was performed for compacts prepared from commercial TZ-3Y-E grade powder. The electron energy was 1.4 MeV. The samples were sintered in the temperature range of 1200–1400 °C. Sintering of zirconia ceramics by high-energy accelerated electron beam is shown to reduce the firing temperature by about 200 °C compared to that in conventional heating technique. Ceramics sintered by accelerated electron beam at 1200 °C is of high density, microhardness and smaller grain size compared to that produced by thermal firing at 1400 °C. Electron beam sintering at higher temperature causes deterioration of ceramics properties due to radiation-induced acceleration of high-temperature recrystallization at higher temperatures.",

keywords = "Grain size, Hardness, High-energy electron beam sintering, Zro",

author = "Surzhikov, {Anatoly Petrovich} and Frangulyan, {T. S.} and Ghyngazov, {S. A.} and Vasil'ev, {I. P.} and Chernyavskii, {Alexander Victorovich}",

year = "2016",

month = sep,

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doi = "10.1016/j.ceramint.2016.05.198",

language = "English",

volume = "42",

pages = "13888--13892",

journal = "Ceramics International",

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publisher = "Elsevier Limited",

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T1 - Sintering of zirconia ceramics by intense high-energy electron beam

AU - Surzhikov, Anatoly Petrovich

AU - Frangulyan, T. S.

AU - Ghyngazov, S. A.

AU - Vasil'ev, I. P.

AU - Chernyavskii, Alexander Victorovich

PY - 2016/9/1

Y1 - 2016/9/1

N2 - A comparative analysis of the efficiency of zirconia ceramics sintering by thermal method and high-energy electron beam sintering was performed for compacts prepared from commercial TZ-3Y-E grade powder. The electron energy was 1.4 MeV. The samples were sintered in the temperature range of 1200–1400 °C. Sintering of zirconia ceramics by high-energy accelerated electron beam is shown to reduce the firing temperature by about 200 °C compared to that in conventional heating technique. Ceramics sintered by accelerated electron beam at 1200 °C is of high density, microhardness and smaller grain size compared to that produced by thermal firing at 1400 °C. Electron beam sintering at higher temperature causes deterioration of ceramics properties due to radiation-induced acceleration of high-temperature recrystallization at higher temperatures.

AB - A comparative analysis of the efficiency of zirconia ceramics sintering by thermal method and high-energy electron beam sintering was performed for compacts prepared from commercial TZ-3Y-E grade powder. The electron energy was 1.4 MeV. The samples were sintered in the temperature range of 1200–1400 °C. Sintering of zirconia ceramics by high-energy accelerated electron beam is shown to reduce the firing temperature by about 200 °C compared to that in conventional heating technique. Ceramics sintered by accelerated electron beam at 1200 °C is of high density, microhardness and smaller grain size compared to that produced by thermal firing at 1400 °C. Electron beam sintering at higher temperature causes deterioration of ceramics properties due to radiation-induced acceleration of high-temperature recrystallization at higher temperatures.

KW - Grain size

KW - Hardness

KW - High-energy electron beam sintering

KW - Zro

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DO - 10.1016/j.ceramint.2016.05.198

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EP - 13892

JO - Ceramics International

JF - Ceramics International

SN - 0272-8842

IS - 12

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