Plasma dynamic synthesis and obtaining ultradispersed zinc oxide with single-crystalline particle structure

Research output: Contribution to journalArticle

13 Citations (Scopus)

Abstract

Zinc oxide is well-known semiconductor material having good electrical, optical and catalytic properties. This paper shows the results on synthesis of hexagonal zinc oxide with single-crystalline particle structure using the system based on coaxial magnetoplasma accelerator. The synthesis is implemented during one short cycle (up to 10−3 s) of plasma accelerator work. X-ray diffractometry analysis allow us to confirm that the product consists of only hexagonal zinc oxide with lattice parameters a = b = 3.24970 Å, c = 5.20270 Å. This result is in a good agreement with EDAX data, which show the presence only Zn and O elements in the final product. SEM, TEM and HRTEM methods are used to investigate the particles morphology. It is found that the product consists of single-crystalline hexagonal particles of zinc oxide and electron diffraction from particles also confirmed the zinc oxide structure. The particle sizes are up to 350 nm but the most of the particles (85%) are less than 150 nm.

Original languageEnglish
Pages (from-to)1506-1513
Number of pages8
JournalAdvanced Powder Technology
Volume27
Issue number4
DOIs
Publication statusPublished - 1 Jul 2016

Fingerprint

Zinc Oxide
Zinc oxide
Crystalline materials
Plasmas
Plasma accelerators
Magnetoplasma
Electron diffraction
X ray diffraction analysis
Lattice constants
Particle accelerators
Energy dispersive spectroscopy
Particle size
Semiconductor materials
Transmission electron microscopy
Scanning electron microscopy

Keywords

  • Hexagonal zinc oxide
  • Nanoparticles
  • Plasma accelerator
  • Single-crystalline particle structure
  • Synthesis

ASJC Scopus subject areas

  • Chemical Engineering(all)
  • Mechanics of Materials

Cite this

@article{bafcbad9e49d431a9274c3feaff24de6,
title = "Plasma dynamic synthesis and obtaining ultradispersed zinc oxide with single-crystalline particle structure",
abstract = "Zinc oxide is well-known semiconductor material having good electrical, optical and catalytic properties. This paper shows the results on synthesis of hexagonal zinc oxide with single-crystalline particle structure using the system based on coaxial magnetoplasma accelerator. The synthesis is implemented during one short cycle (up to 10−3 s) of plasma accelerator work. X-ray diffractometry analysis allow us to confirm that the product consists of only hexagonal zinc oxide with lattice parameters a = b = 3.24970 {\AA}, c = 5.20270 {\AA}. This result is in a good agreement with EDAX data, which show the presence only Zn and O elements in the final product. SEM, TEM and HRTEM methods are used to investigate the particles morphology. It is found that the product consists of single-crystalline hexagonal particles of zinc oxide and electron diffraction from particles also confirmed the zinc oxide structure. The particle sizes are up to 350 nm but the most of the particles (85{\%}) are less than 150 nm.",
keywords = "Hexagonal zinc oxide, Nanoparticles, Plasma accelerator, Single-crystalline particle structure, Synthesis",
author = "Alexander Sivkov and Alexander Ivashutenko and Yuliya Shanenkova and Ivan Shanenkov",
year = "2016",
month = "7",
day = "1",
doi = "10.1016/j.apt.2016.05.012",
language = "English",
volume = "27",
pages = "1506--1513",
journal = "Advanced Powder Technology",
issn = "0921-8831",
publisher = "Elsevier BV",
number = "4",

}

TY - JOUR

T1 - Plasma dynamic synthesis and obtaining ultradispersed zinc oxide with single-crystalline particle structure

AU - Sivkov, Alexander

AU - Ivashutenko, Alexander

AU - Shanenkova, Yuliya

AU - Shanenkov, Ivan

PY - 2016/7/1

Y1 - 2016/7/1

N2 - Zinc oxide is well-known semiconductor material having good electrical, optical and catalytic properties. This paper shows the results on synthesis of hexagonal zinc oxide with single-crystalline particle structure using the system based on coaxial magnetoplasma accelerator. The synthesis is implemented during one short cycle (up to 10−3 s) of plasma accelerator work. X-ray diffractometry analysis allow us to confirm that the product consists of only hexagonal zinc oxide with lattice parameters a = b = 3.24970 Å, c = 5.20270 Å. This result is in a good agreement with EDAX data, which show the presence only Zn and O elements in the final product. SEM, TEM and HRTEM methods are used to investigate the particles morphology. It is found that the product consists of single-crystalline hexagonal particles of zinc oxide and electron diffraction from particles also confirmed the zinc oxide structure. The particle sizes are up to 350 nm but the most of the particles (85%) are less than 150 nm.

AB - Zinc oxide is well-known semiconductor material having good electrical, optical and catalytic properties. This paper shows the results on synthesis of hexagonal zinc oxide with single-crystalline particle structure using the system based on coaxial magnetoplasma accelerator. The synthesis is implemented during one short cycle (up to 10−3 s) of plasma accelerator work. X-ray diffractometry analysis allow us to confirm that the product consists of only hexagonal zinc oxide with lattice parameters a = b = 3.24970 Å, c = 5.20270 Å. This result is in a good agreement with EDAX data, which show the presence only Zn and O elements in the final product. SEM, TEM and HRTEM methods are used to investigate the particles morphology. It is found that the product consists of single-crystalline hexagonal particles of zinc oxide and electron diffraction from particles also confirmed the zinc oxide structure. The particle sizes are up to 350 nm but the most of the particles (85%) are less than 150 nm.

KW - Hexagonal zinc oxide

KW - Nanoparticles

KW - Plasma accelerator

KW - Single-crystalline particle structure

KW - Synthesis

UR - http://www.scopus.com/inward/record.url?scp=84976520410&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=84976520410&partnerID=8YFLogxK

U2 - 10.1016/j.apt.2016.05.012

DO - 10.1016/j.apt.2016.05.012

M3 - Article

AN - SCOPUS:84976520410

VL - 27

SP - 1506

EP - 1513

JO - Advanced Powder Technology

JF - Advanced Powder Technology

SN - 0921-8831

IS - 4

ER -