Phase composition and pore structure of nanoparticulate tin oxides prepared by AC electrochemical synthesis

V. V. Korobochkin, M. A. Balmashnov, D. A. Gorlushko, Natalia Vasilievna Usoltseva, V. V. Bochkareva

Research output: Contribution to journalArticle

2 Citations (Scopus)

Abstract

The effect of current density and sodium chloride concentration in solution on the phase composition and pore structure of the products of ac electrolysis of metallic Sn has been studied using X-ray diffraction, thermogravimetry, differential scanning calorimetry, electron microscopy, and low-temperature nitrogen adsorption measurements. The results demonstrate that the synthesis products consist of tin(II) and tin(IV) oxides and hydroxides, whose percentages depend on electrolysis conditions, and have a large specific surface area and mesoporous structure. The average particle size ranges from 10 to 30 nm.

Original languageEnglish
Pages (from-to)993-999
Number of pages7
JournalInorganic Materials
Volume49
Issue number10
DOIs
Publication statusPublished - Oct 2013

Fingerprint

Pore structure
Tin oxides
Electrolysis
Phase composition
Hydroxides
Tin
Sodium chloride
Sodium Chloride
Specific surface area
Electron microscopy
Thermogravimetric analysis
Differential scanning calorimetry
Current density
Nitrogen
Particle size
Adsorption
X ray diffraction
Temperature
stannic oxide

ASJC Scopus subject areas

  • Inorganic Chemistry
  • Chemical Engineering(all)
  • Materials Chemistry
  • Metals and Alloys

Cite this

Phase composition and pore structure of nanoparticulate tin oxides prepared by AC electrochemical synthesis. / Korobochkin, V. V.; Balmashnov, M. A.; Gorlushko, D. A.; Usoltseva, Natalia Vasilievna; Bochkareva, V. V.

In: Inorganic Materials, Vol. 49, No. 10, 10.2013, p. 993-999.

Research output: Contribution to journalArticle

@article{39e21e3b43574c53a80a0519942a2e7e,
title = "Phase composition and pore structure of nanoparticulate tin oxides prepared by AC electrochemical synthesis",
abstract = "The effect of current density and sodium chloride concentration in solution on the phase composition and pore structure of the products of ac electrolysis of metallic Sn has been studied using X-ray diffraction, thermogravimetry, differential scanning calorimetry, electron microscopy, and low-temperature nitrogen adsorption measurements. The results demonstrate that the synthesis products consist of tin(II) and tin(IV) oxides and hydroxides, whose percentages depend on electrolysis conditions, and have a large specific surface area and mesoporous structure. The average particle size ranges from 10 to 30 nm.",
author = "Korobochkin, {V. V.} and Balmashnov, {M. A.} and Gorlushko, {D. A.} and Usoltseva, {Natalia Vasilievna} and Bochkareva, {V. V.}",
year = "2013",
month = "10",
doi = "10.1134/S0020168513100051",
language = "English",
volume = "49",
pages = "993--999",
journal = "Inorganic Materials",
issn = "0020-1685",
publisher = "Maik Nauka-Interperiodica Publishing",
number = "10",

}

TY - JOUR

T1 - Phase composition and pore structure of nanoparticulate tin oxides prepared by AC electrochemical synthesis

AU - Korobochkin, V. V.

AU - Balmashnov, M. A.

AU - Gorlushko, D. A.

AU - Usoltseva, Natalia Vasilievna

AU - Bochkareva, V. V.

PY - 2013/10

Y1 - 2013/10

N2 - The effect of current density and sodium chloride concentration in solution on the phase composition and pore structure of the products of ac electrolysis of metallic Sn has been studied using X-ray diffraction, thermogravimetry, differential scanning calorimetry, electron microscopy, and low-temperature nitrogen adsorption measurements. The results demonstrate that the synthesis products consist of tin(II) and tin(IV) oxides and hydroxides, whose percentages depend on electrolysis conditions, and have a large specific surface area and mesoporous structure. The average particle size ranges from 10 to 30 nm.

AB - The effect of current density and sodium chloride concentration in solution on the phase composition and pore structure of the products of ac electrolysis of metallic Sn has been studied using X-ray diffraction, thermogravimetry, differential scanning calorimetry, electron microscopy, and low-temperature nitrogen adsorption measurements. The results demonstrate that the synthesis products consist of tin(II) and tin(IV) oxides and hydroxides, whose percentages depend on electrolysis conditions, and have a large specific surface area and mesoporous structure. The average particle size ranges from 10 to 30 nm.

UR - http://www.scopus.com/inward/record.url?scp=84883690889&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=84883690889&partnerID=8YFLogxK

U2 - 10.1134/S0020168513100051

DO - 10.1134/S0020168513100051

M3 - Article

VL - 49

SP - 993

EP - 999

JO - Inorganic Materials

JF - Inorganic Materials

SN - 0020-1685

IS - 10

ER -