Abstract
Alloy of the V-Ti-Cr system is a promising material exploited under high radiation and in corrosion environment. We sintered V-4.9Ti-4.8Cr alloy from particles with original average size of 30, 280 and 200 μm, respectively for vanadium, titanium and chromium powders, by pressing of the powder mixture and its further sintering. The studies were undertaken using the methods of X-ray structural analysis, scanning electron microscopy with an energy dispersive analyzer and transmission electron microscopy. It was established that the structure of the alloy represented matrix grains (BCC solid solution), along the boundaries and at junctions of which the groups of oxycarbonitride particles of V, Ti, Cr (C,N,O) type of the variable elemental composition were arranged. The particles possessed a plate-like (0.4 x 2.0 μm) and rounded (0.5 μm) shape. The solid solution of the alloy was heterogeneous by concentration. This was evidenced by the complications of the diffraction patterns obtained from the corresponding sections of the structure. These were cords of main reflexes, satellites and emergence of a moire banded contrast in separate sections of the sample. Inside the matrix grains, there were nanoparticles (15 μm) of carbide V55Cr25C20, being a source of elastic internal local stresses.
| Original language | English |
|---|---|
| Article number | 012051 |
| Journal | Journal of Physics: Conference Series |
| Volume | 1145 |
| Issue number | 1 |
| DOIs | |
| Publication status | Published - 9 Jan 2019 |
| Event | 15th International Conference of Students and Young Scientists on Prospects of Fundamental Sciences Development, PFSD 2018 - Tomsk, Russian Federation Duration: 24 Apr 2018 → 27 Apr 2018 |
Fingerprint
ASJC Scopus subject areas
- Physics and Astronomy(all)
Cite this
Peculiarities of structure and phase composition of V-Ti-Cr alloy obtained by sintering technique. / Kurzina, I.; Popova, N.; Kalashnikov, M.; Nikonenko, E.; Kazantseva, L.; Dement, T.; Klopotov, A.; Abzaev, Yu; Karakchieva, N.; Koneva, N.
In: Journal of Physics: Conference Series, Vol. 1145, No. 1, 012051, 09.01.2019.Research output: Contribution to journal › Conference article
}
TY - JOUR
T1 - Peculiarities of structure and phase composition of V-Ti-Cr alloy obtained by sintering technique
AU - Kurzina, I.
AU - Popova, N.
AU - Kalashnikov, M.
AU - Nikonenko, E.
AU - Kazantseva, L.
AU - Dement, T.
AU - Klopotov, A.
AU - Abzaev, Yu
AU - Karakchieva, N.
AU - Koneva, N.
PY - 2019/1/9
Y1 - 2019/1/9
N2 - Alloy of the V-Ti-Cr system is a promising material exploited under high radiation and in corrosion environment. We sintered V-4.9Ti-4.8Cr alloy from particles with original average size of 30, 280 and 200 μm, respectively for vanadium, titanium and chromium powders, by pressing of the powder mixture and its further sintering. The studies were undertaken using the methods of X-ray structural analysis, scanning electron microscopy with an energy dispersive analyzer and transmission electron microscopy. It was established that the structure of the alloy represented matrix grains (BCC solid solution), along the boundaries and at junctions of which the groups of oxycarbonitride particles of V, Ti, Cr (C,N,O) type of the variable elemental composition were arranged. The particles possessed a plate-like (0.4 x 2.0 μm) and rounded (0.5 μm) shape. The solid solution of the alloy was heterogeneous by concentration. This was evidenced by the complications of the diffraction patterns obtained from the corresponding sections of the structure. These were cords of main reflexes, satellites and emergence of a moire banded contrast in separate sections of the sample. Inside the matrix grains, there were nanoparticles (15 μm) of carbide V55Cr25C20, being a source of elastic internal local stresses.
AB - Alloy of the V-Ti-Cr system is a promising material exploited under high radiation and in corrosion environment. We sintered V-4.9Ti-4.8Cr alloy from particles with original average size of 30, 280 and 200 μm, respectively for vanadium, titanium and chromium powders, by pressing of the powder mixture and its further sintering. The studies were undertaken using the methods of X-ray structural analysis, scanning electron microscopy with an energy dispersive analyzer and transmission electron microscopy. It was established that the structure of the alloy represented matrix grains (BCC solid solution), along the boundaries and at junctions of which the groups of oxycarbonitride particles of V, Ti, Cr (C,N,O) type of the variable elemental composition were arranged. The particles possessed a plate-like (0.4 x 2.0 μm) and rounded (0.5 μm) shape. The solid solution of the alloy was heterogeneous by concentration. This was evidenced by the complications of the diffraction patterns obtained from the corresponding sections of the structure. These were cords of main reflexes, satellites and emergence of a moire banded contrast in separate sections of the sample. Inside the matrix grains, there were nanoparticles (15 μm) of carbide V55Cr25C20, being a source of elastic internal local stresses.
UR - http://www.scopus.com/inward/record.url?scp=85060049922&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=85060049922&partnerID=8YFLogxK
U2 - 10.1088/1742-6596/1145/1/012051
DO - 10.1088/1742-6596/1145/1/012051
M3 - Conference article
VL - 1145
JO - Journal of Physics: Conference Series
JF - Journal of Physics: Conference Series
SN - 1742-6588
IS - 1
M1 - 012051
ER -