One-pot amide synthesis via thermal decomposition N-acylureas under microwave irradiation

N. S. Soldatova, K. V. Orlova, T. A. Sarycheva

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Abstract

A simple one-pot amidation of carboxylic acids promoted by microwave irradiation is described. Reaction includes formation N-acylureas via interaction carboxylic acids and N,Ndicyclohexylcarbodiimide followed thermal decomposition N-acylureas in microwave reactor. This method allows carrying out the reaction in a short time with good yields.

Original language	English
Title of host publication	High Technology
Subtitle of host publication	Research and Applications, 2015
Editors	Nikita Martyushev, Anna Bogdan
Publisher	Trans Tech Publications Ltd
Pages	785-788
Number of pages	4
ISBN (Print)	9783038357087
DOIs	https://doi.org/10.4028/www.scientific.net/KEM.685.785
Publication status	Published - 1 Jan 2016
Event	4th International Conference for Young Scientists High Technology: Research and Applications, HTRA 2015 - Tomsk, Russian Federation Duration: 21 Apr 2015 → 24 Apr 2015

Publication series

Name	Key Engineering Materials
Volume	685
ISSN (Print)	1013-9826

Conference

Conference	4th International Conference for Young Scientists High Technology: Research and Applications, HTRA 2015
Country	Russian Federation
City	Tomsk
Period	21.4.15 → 24.4.15

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Keywords

Amidation
Carbodiimides
Microwave irradiation
N-acylureas

ASJC Scopus subject areas

Materials Science(all)
Mechanics of Materials
Mechanical Engineering

Cite this

Soldatova, N. S., Orlova, K. V., & Sarycheva, T. A. (2016). One-pot amide synthesis via thermal decomposition N-acylureas under microwave irradiation. In N. Martyushev, & A. Bogdan (Eds.), High Technology: Research and Applications, 2015 (pp. 785-788). (Key Engineering Materials; Vol. 685). Trans Tech Publications Ltd. https://doi.org/10.4028/www.scientific.net/KEM.685.785

One-pot amide synthesis via thermal decomposition N-acylureas under microwave irradiation. / Soldatova, N. S.; Orlova, K. V.; Sarycheva, T. A.

High Technology: Research and Applications, 2015. ed. / Nikita Martyushev; Anna Bogdan. Trans Tech Publications Ltd, 2016. p. 785-788 (Key Engineering Materials; Vol. 685).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Soldatova, NS , Orlova, KV & Sarycheva, TA 2016, One-pot amide synthesis via thermal decomposition N-acylureas under microwave irradiation. in N Martyushev & A Bogdan (eds), High Technology: Research and Applications, 2015. Key Engineering Materials, vol. 685, Trans Tech Publications Ltd, pp. 785-788, 4th International Conference for Young Scientists High Technology: Research and Applications, HTRA 2015, Tomsk, Russian Federation, 21.4.15. https://doi.org/10.4028/www.scientific.net/KEM.685.785

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Access to Document

10.4028/www.scientific.net/KEM.685.785