Abstract
This paper reports the influence of microwave treatment duration and pH conditions of initial precursors on the morphological and crystalline dispersity of the hydroxyapatite (HAp) synthesized by hydrothermal method.The obtained HAp samples were studied by scanning electron microscopy, X-Ray diffraction method and low nitrogen adsorption method. We have obtained nanostructured crystalline hydroxyapatite with 95% crystallinity, porous structure and average particles size in interval 17...46 nm consolidated in aggregates with size distribution of 0.5...25 μm. The pH growth from 8 to 13 results in double increase of HAp specific area(from 69 up to 133 m2/g), meanwhile microwave irradiation brings to particles aggregation: HAp treated during 0... 10...30 min have specific surface are 112...67...41 m2/g, respectively. As a result at pH=13 and without microwave irradiation treatment we synthesized HAp with maximum surface compared to the surface of natural HAp that makes obtained HApto be promising material in biotechnological applications.
| Original language | English |
|---|---|
| Article number | 012003 |
| Journal | Journal of Physics: Conference Series |
| Volume | 1145 |
| Issue number | 1 |
| DOIs | |
| Publication status | Published - 9 Jan 2019 |
| Event | 15th International Conference of Students and Young Scientists on Prospects of Fundamental Sciences Development, PFSD 2018 - Tomsk, Russian Federation Duration: 24 Apr 2018 → 27 Apr 2018 |
Fingerprint
ASJC Scopus subject areas
- Physics and Astronomy(all)
Cite this
Microwave treatment and pH influence on hydroxyapatite morphology and structure. / Yudin, A.; Ilinykh, I.; Chuprunov, K.; Kolesnikov, E.; Kuznetsov, D.; Leybo, D.; Godymchuk, A.
In: Journal of Physics: Conference Series, Vol. 1145, No. 1, 012003, 09.01.2019.Research output: Contribution to journal › Conference article
}
TY - JOUR
T1 - Microwave treatment and pH influence on hydroxyapatite morphology and structure
AU - Yudin, A.
AU - Ilinykh, I.
AU - Chuprunov, K.
AU - Kolesnikov, E.
AU - Kuznetsov, D.
AU - Leybo, D.
AU - Godymchuk, A.
PY - 2019/1/9
Y1 - 2019/1/9
N2 - This paper reports the influence of microwave treatment duration and pH conditions of initial precursors on the morphological and crystalline dispersity of the hydroxyapatite (HAp) synthesized by hydrothermal method.The obtained HAp samples were studied by scanning electron microscopy, X-Ray diffraction method and low nitrogen adsorption method. We have obtained nanostructured crystalline hydroxyapatite with 95% crystallinity, porous structure and average particles size in interval 17...46 nm consolidated in aggregates with size distribution of 0.5...25 μm. The pH growth from 8 to 13 results in double increase of HAp specific area(from 69 up to 133 m2/g), meanwhile microwave irradiation brings to particles aggregation: HAp treated during 0... 10...30 min have specific surface are 112...67...41 m2/g, respectively. As a result at pH=13 and without microwave irradiation treatment we synthesized HAp with maximum surface compared to the surface of natural HAp that makes obtained HApto be promising material in biotechnological applications.
AB - This paper reports the influence of microwave treatment duration and pH conditions of initial precursors on the morphological and crystalline dispersity of the hydroxyapatite (HAp) synthesized by hydrothermal method.The obtained HAp samples were studied by scanning electron microscopy, X-Ray diffraction method and low nitrogen adsorption method. We have obtained nanostructured crystalline hydroxyapatite with 95% crystallinity, porous structure and average particles size in interval 17...46 nm consolidated in aggregates with size distribution of 0.5...25 μm. The pH growth from 8 to 13 results in double increase of HAp specific area(from 69 up to 133 m2/g), meanwhile microwave irradiation brings to particles aggregation: HAp treated during 0... 10...30 min have specific surface are 112...67...41 m2/g, respectively. As a result at pH=13 and without microwave irradiation treatment we synthesized HAp with maximum surface compared to the surface of natural HAp that makes obtained HApto be promising material in biotechnological applications.
UR - http://www.scopus.com/inward/record.url?scp=85060021184&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=85060021184&partnerID=8YFLogxK
U2 - 10.1088/1742-6596/1145/1/012003
DO - 10.1088/1742-6596/1145/1/012003
M3 - Conference article
AN - SCOPUS:85060021184
VL - 1145
JO - Journal of Physics: Conference Series
JF - Journal of Physics: Conference Series
SN - 1742-6588
IS - 1
M1 - 012003
ER -