Abstract
A comparative investigation of microstructure, mechanical and biological properties for zirconium alloyed with niobium in coarse-grained and ultra-fine grained states is presented. The temperature and deformation regimes of multi-stage abc-pressing resulted in ultra-fine grained states with an average size of the structural elements in the range of 0.28-0.55 μm, depending on the accumulated strain during pressing. The increase of the accumulated strain at each stage of pressing increased the uniformity of the structure. The microhardness increased by 50% with increased accumulated strain during the severe plastic deformation. Between the microhardness and the average size of the structural elements, a linear dependence was found, indicating a Hall-Petch relationship. The alloy had a good biocompatibility as shown by an MTT test with osteoblasts (MG-63 cell line). The good mechanical properties (microhardness) of zirconium alloyed with niobium in the ultra-fine grained state make it suitable for medical applications, e. g. as implant material.
| Original language | English |
|---|---|
| Pages (from-to) | 198-204 |
| Number of pages | 7 |
| Journal | Materialwissenschaft und Werkstofftechnik |
| Volume | 44 |
| Issue number | 2-3 |
| DOIs | |
| Publication status | Published - Feb 2013 |
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Keywords
- alloys
- biomaterials
- mechanical properties
- microstructure
- plastic deformation
ASJC Scopus subject areas
- Materials Science(all)
- Condensed Matter Physics
- Mechanical Engineering
- Mechanics of Materials
Cite this
Microstructure, mechanical and biological properties of zirconium alloyed with niobium after severe plastic deformation. / Sharkeev, Y. P.; Eroshenko, A. Y.; Kulyashova, K. S.; Fortuna, S. V.; Suvorov, K. A.; Epple, M.; Prymak, O.; Sokolova, V.; Chernousova, S.
In: Materialwissenschaft und Werkstofftechnik, Vol. 44, No. 2-3, 02.2013, p. 198-204.Research output: Contribution to journal › Article
}
TY - JOUR
T1 - Microstructure, mechanical and biological properties of zirconium alloyed with niobium after severe plastic deformation
AU - Sharkeev, Y. P.
AU - Eroshenko, A. Y.
AU - Kulyashova, K. S.
AU - Fortuna, S. V.
AU - Suvorov, K. A.
AU - Epple, M.
AU - Prymak, O.
AU - Sokolova, V.
AU - Chernousova, S.
PY - 2013/2
Y1 - 2013/2
N2 - A comparative investigation of microstructure, mechanical and biological properties for zirconium alloyed with niobium in coarse-grained and ultra-fine grained states is presented. The temperature and deformation regimes of multi-stage abc-pressing resulted in ultra-fine grained states with an average size of the structural elements in the range of 0.28-0.55 μm, depending on the accumulated strain during pressing. The increase of the accumulated strain at each stage of pressing increased the uniformity of the structure. The microhardness increased by 50% with increased accumulated strain during the severe plastic deformation. Between the microhardness and the average size of the structural elements, a linear dependence was found, indicating a Hall-Petch relationship. The alloy had a good biocompatibility as shown by an MTT test with osteoblasts (MG-63 cell line). The good mechanical properties (microhardness) of zirconium alloyed with niobium in the ultra-fine grained state make it suitable for medical applications, e. g. as implant material.
AB - A comparative investigation of microstructure, mechanical and biological properties for zirconium alloyed with niobium in coarse-grained and ultra-fine grained states is presented. The temperature and deformation regimes of multi-stage abc-pressing resulted in ultra-fine grained states with an average size of the structural elements in the range of 0.28-0.55 μm, depending on the accumulated strain during pressing. The increase of the accumulated strain at each stage of pressing increased the uniformity of the structure. The microhardness increased by 50% with increased accumulated strain during the severe plastic deformation. Between the microhardness and the average size of the structural elements, a linear dependence was found, indicating a Hall-Petch relationship. The alloy had a good biocompatibility as shown by an MTT test with osteoblasts (MG-63 cell line). The good mechanical properties (microhardness) of zirconium alloyed with niobium in the ultra-fine grained state make it suitable for medical applications, e. g. as implant material.
KW - alloys
KW - biomaterials
KW - mechanical properties
KW - microstructure
KW - plastic deformation
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UR - http://www.scopus.com/inward/citedby.url?scp=84875250587&partnerID=8YFLogxK
U2 - 10.1002/mawe.201300113
DO - 10.1002/mawe.201300113
M3 - Article
AN - SCOPUS:84875250587
VL - 44
SP - 198
EP - 204
JO - Materialwissenschaft und Werkstofftechnik
JF - Materialwissenschaft und Werkstofftechnik
SN - 0933-5137
IS - 2-3
ER -