Influence of the degree of compaction of a reagent powder mixture on solid-phase synthesis of lithium pentaferrite

A. M. Pritulov, R. U. Usmanov, O. V. Gal'Tseva, A. A. Kondratyuk, V. V. Bezuglov, V. I. Serbin

Research output: Contribution to journalArticle

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Abstract

Interrelation between the compaction pressure of lithium carbonate and iron oxide powder mixture and efficiency of solid-phase synthesis of lithium pentaferrite are investigated. It is demonstrated that the temperature dependence of the degree of transformation during isochronous annealing for 60 min obeys the Arrhenius law. The effective activation energy of the process decreases when the compaction pressure increases from 0.4 (P = 0) to 0.2 eV (P = 202 MPa). A linear dependence between the degree of transformation and the specific magnetization of the mixture is observed at synthesis temperatures of 870-1070 K. No influence of the compaction pressure on the magnetic anisotropy field of synthesized spinel is revealed.

Original languageEnglish
Pages (from-to)187-192
Number of pages6
JournalRussian Physics Journal
Volume50
Issue number2
DOIs
Publication statusPublished - 1 Feb 2007

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reagents
solid phases
lithium
synthesis
iron oxides
spinel
carbonates
activation energy
magnetization
temperature dependence
anisotropy
annealing
oxides
temperature

ASJC Scopus subject areas

  • Physics and Astronomy(all)

Cite this

Influence of the degree of compaction of a reagent powder mixture on solid-phase synthesis of lithium pentaferrite. / Pritulov, A. M.; Usmanov, R. U.; Gal'Tseva, O. V.; Kondratyuk, A. A.; Bezuglov, V. V.; Serbin, V. I.

In: Russian Physics Journal, Vol. 50, No. 2, 01.02.2007, p. 187-192.

Research output: Contribution to journalArticle

Pritulov, A. M. ; Usmanov, R. U. ; Gal'Tseva, O. V. ; Kondratyuk, A. A. ; Bezuglov, V. V. ; Serbin, V. I. / Influence of the degree of compaction of a reagent powder mixture on solid-phase synthesis of lithium pentaferrite. In: Russian Physics Journal. 2007 ; Vol. 50, No. 2. pp. 187-192.
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