In Situ Investigation of Thermo-stimulated Decay of Hydrides of Titanium and Zirconium by Means of X-ray Diffraction of Synchrotron Radiation

Roman S. Laptev, Maxim S. Syrtanov, Viktor N. Kudiiarov, Alexander N. Shmakov, Zakhar S. Vinokurov, Andrey A. Mikhaylov, Konstantin V. Zolotarev

Research output: Contribution to journalArticle

3 Citations (Scopus)

Abstract

Titanium and zirconium are used in many fields such as chemical, aircraft and nuclear industries. Hydrogen penetration and accumulation in titanium and zirconium alloys leads to the hydrogen-induced embrittlement. The study of hydrogen accumulation and distribution as well as phase transitions in zirconium alloy Zr1%Nb and commercially pure titanium alloy during the gas-phase hydrogenation is motivated by looking for a way to prevent materials from embrittlement. Gas-phase hydrogenation and thermo-stimulated desorption methods were used for hydrogen sorption and accumulation processes investigation. Synchrotron XRD method was applied for in situ investigation of phase transitions during heating of hydrogen saturated materials. Measurements were performed using SR from the VEPP-3 storage ring.

Original languageEnglish
Pages (from-to)337-341
Number of pages5
JournalPhysics Procedia
Volume84
DOIs
Publication statusPublished - 2016
EventInternational Conference on Synchrotron and Free Electron Laser Radiation: Generation and Application, SFR 2016 - Novosibirsk, Russian Federation
Duration: 4 Jul 20167 Jul 2016

Fingerprint

hydrides
synchrotron radiation
titanium
zirconium alloys
decay
hydrogen
diffraction
embrittlement
titanium alloys
x rays
hydrogenation
aircraft industry
industries
vapor phases
sorption
synchrotrons
penetration
desorption
heating

Keywords

  • hydrogen sorption curves
  • hydrogenation
  • phase transitions
  • synchrotron radiation
  • zirconium alloy

ASJC Scopus subject areas

  • Physics and Astronomy(all)

Cite this

In Situ Investigation of Thermo-stimulated Decay of Hydrides of Titanium and Zirconium by Means of X-ray Diffraction of Synchrotron Radiation. / Laptev, Roman S.; Syrtanov, Maxim S.; Kudiiarov, Viktor N.; Shmakov, Alexander N.; Vinokurov, Zakhar S.; Mikhaylov, Andrey A.; Zolotarev, Konstantin V.

In: Physics Procedia, Vol. 84, 2016, p. 337-341.

Research output: Contribution to journalArticle

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AU - Syrtanov, Maxim S.

AU - Kudiiarov, Viktor N.

AU - Shmakov, Alexander N.

AU - Vinokurov, Zakhar S.

AU - Mikhaylov, Andrey A.

AU - Zolotarev, Konstantin V.

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N2 - Titanium and zirconium are used in many fields such as chemical, aircraft and nuclear industries. Hydrogen penetration and accumulation in titanium and zirconium alloys leads to the hydrogen-induced embrittlement. The study of hydrogen accumulation and distribution as well as phase transitions in zirconium alloy Zr1%Nb and commercially pure titanium alloy during the gas-phase hydrogenation is motivated by looking for a way to prevent materials from embrittlement. Gas-phase hydrogenation and thermo-stimulated desorption methods were used for hydrogen sorption and accumulation processes investigation. Synchrotron XRD method was applied for in situ investigation of phase transitions during heating of hydrogen saturated materials. Measurements were performed using SR from the VEPP-3 storage ring.

AB - Titanium and zirconium are used in many fields such as chemical, aircraft and nuclear industries. Hydrogen penetration and accumulation in titanium and zirconium alloys leads to the hydrogen-induced embrittlement. The study of hydrogen accumulation and distribution as well as phase transitions in zirconium alloy Zr1%Nb and commercially pure titanium alloy during the gas-phase hydrogenation is motivated by looking for a way to prevent materials from embrittlement. Gas-phase hydrogenation and thermo-stimulated desorption methods were used for hydrogen sorption and accumulation processes investigation. Synchrotron XRD method was applied for in situ investigation of phase transitions during heating of hydrogen saturated materials. Measurements were performed using SR from the VEPP-3 storage ring.

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