Hydrogen calibration of GD-spectrometer using Zr-1Nb alloy

Andrey A. Mikhaylov, Tatiana S. Priamushko, Maria N. Babikhina, Victor N. Kudiiarov, Rene Heller, Roman S. Laptev, Andrey M. Lider

Research output: Contribution to journalArticle

1 Citation (Scopus)

Abstract

To study the hydrogen distribution in Zr-1Nb alloy (E(cyrillic)110 alloy) GD-OES was applied in this work. Qualitative analysis needs the standard samples with hydrogen. However, the standard samples with high concentrations of hydrogen in the zirconium alloy which would meet the requirements of the shape, size are absent. In this work method of Zr + H calibration samples production was performed at the first time. Automated Complex Gas Reaction Controller was used for samples hydrogenation. To calculate the parameters of post-hydrogenation incubation of the samples in an inert gas atmosphere the diffusion equations were used. Absolute hydrogen concentrations in the samples were determined by melting in the inert gas atmosphere using RHEN602 analyzer (LECO Company). Hydrogen distribution was studied using nuclear reaction analysis (HZDR, Dresden, Germany). RF GD-OES was used for calibration. The depth of the craters was measured with the help of a Hommel-Etamic profilometer by Jenoptik, Germany.

Original languageEnglish
JournalApplied Surface Science
DOIs
Publication statusAccepted/In press - 31 Oct 2016

Fingerprint

Spectrometers
Hydrogen
Calibration
Noble Gases
Inert gases
Hydrogenation
Zirconium alloys
Nuclear reactions
Melting
Gases
Controllers
Industry

Keywords

  • Calibration
  • Glow discharge optical emission spectroscopy (GD-OES)
  • Hydrogen
  • Standard samples
  • Zirconium alloy

ASJC Scopus subject areas

  • Surfaces, Coatings and Films

Cite this

Hydrogen calibration of GD-spectrometer using Zr-1Nb alloy. / Mikhaylov, Andrey A.; Priamushko, Tatiana S.; Babikhina, Maria N.; Kudiiarov, Victor N.; Heller, Rene; Laptev, Roman S.; Lider, Andrey M.

In: Applied Surface Science, 31.10.2016.

Research output: Contribution to journalArticle

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AU - Kudiiarov, Victor N.

AU - Heller, Rene

AU - Laptev, Roman S.

AU - Lider, Andrey M.

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