Abstract
To study the hydrogen distribution in Zr-1Nb alloy (E(cyrillic)110 alloy) GD-OES was applied in this work. Qualitative analysis needs the standard samples with hydrogen. However, the standard samples with high concentrations of hydrogen in the zirconium alloy which would meet the requirements of the shape, size are absent. In this work method of Zr + H calibration samples production was performed at the first time. Automated Complex Gas Reaction Controller was used for samples hydrogenation. To calculate the parameters of post-hydrogenation incubation of the samples in an inert gas atmosphere the diffusion equations were used. Absolute hydrogen concentrations in the samples were determined by melting in the inert gas atmosphere using RHEN602 analyzer (LECO Company). Hydrogen distribution was studied using nuclear reaction analysis (HZDR, Dresden, Germany). RF GD-OES was used for calibration. The depth of the craters was measured with the help of a Hommel-Etamic profilometer by Jenoptik, Germany.
| Original language | English |
|---|---|
| Journal | Applied Surface Science |
| DOIs | |
| Publication status | Accepted/In press - 31 Oct 2016 |
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Keywords
- Calibration
- Glow discharge optical emission spectroscopy (GD-OES)
- Hydrogen
- Standard samples
- Zirconium alloy
ASJC Scopus subject areas
- Surfaces, Coatings and Films
Cite this
Hydrogen calibration of GD-spectrometer using Zr-1Nb alloy. / Mikhaylov, Andrey A.; Priamushko, Tatiana S.; Babikhina, Maria N.; Kudiiarov, Victor N.; Heller, Rene; Laptev, Roman S.; Lider, Andrey M.
In: Applied Surface Science, 31.10.2016.Research output: Contribution to journal › Article
}
TY - JOUR
T1 - Hydrogen calibration of GD-spectrometer using Zr-1Nb alloy
AU - Mikhaylov, Andrey A.
AU - Priamushko, Tatiana S.
AU - Babikhina, Maria N.
AU - Kudiiarov, Victor N.
AU - Heller, Rene
AU - Laptev, Roman S.
AU - Lider, Andrey M.
PY - 2016/10/31
Y1 - 2016/10/31
N2 - To study the hydrogen distribution in Zr-1Nb alloy (E(cyrillic)110 alloy) GD-OES was applied in this work. Qualitative analysis needs the standard samples with hydrogen. However, the standard samples with high concentrations of hydrogen in the zirconium alloy which would meet the requirements of the shape, size are absent. In this work method of Zr + H calibration samples production was performed at the first time. Automated Complex Gas Reaction Controller was used for samples hydrogenation. To calculate the parameters of post-hydrogenation incubation of the samples in an inert gas atmosphere the diffusion equations were used. Absolute hydrogen concentrations in the samples were determined by melting in the inert gas atmosphere using RHEN602 analyzer (LECO Company). Hydrogen distribution was studied using nuclear reaction analysis (HZDR, Dresden, Germany). RF GD-OES was used for calibration. The depth of the craters was measured with the help of a Hommel-Etamic profilometer by Jenoptik, Germany.
AB - To study the hydrogen distribution in Zr-1Nb alloy (E(cyrillic)110 alloy) GD-OES was applied in this work. Qualitative analysis needs the standard samples with hydrogen. However, the standard samples with high concentrations of hydrogen in the zirconium alloy which would meet the requirements of the shape, size are absent. In this work method of Zr + H calibration samples production was performed at the first time. Automated Complex Gas Reaction Controller was used for samples hydrogenation. To calculate the parameters of post-hydrogenation incubation of the samples in an inert gas atmosphere the diffusion equations were used. Absolute hydrogen concentrations in the samples were determined by melting in the inert gas atmosphere using RHEN602 analyzer (LECO Company). Hydrogen distribution was studied using nuclear reaction analysis (HZDR, Dresden, Germany). RF GD-OES was used for calibration. The depth of the craters was measured with the help of a Hommel-Etamic profilometer by Jenoptik, Germany.
KW - Calibration
KW - Glow discharge optical emission spectroscopy (GD-OES)
KW - Hydrogen
KW - Standard samples
KW - Zirconium alloy
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UR - http://www.scopus.com/inward/citedby.url?scp=85021083376&partnerID=8YFLogxK
U2 - 10.1016/j.apsusc.2017.06.191
DO - 10.1016/j.apsusc.2017.06.191
M3 - Article
AN - SCOPUS:85021083376
JO - Applied Surface Science
JF - Applied Surface Science
SN - 0169-4332
ER -