High-yield microwave synthesis of layered Y2(OH)5NO3·xH2O materials

A. D. Yapryntsev, A. E. Baranchikov, L. S. Skogareva, A. E. Goldt, I. P. Stolyarov, O. S. Ivanova, V. V. Kozik, V. K. Ivanov

    Research output: Contribution to journalArticle

    14 Citations (Scopus)

    Abstract

    A novel, facile, and versatile microwave-assisted method of high-yield synthesis of layered rare earth hydroxo compounds (LRHs) is proposed. Layered yttrium hydroxonitrates synthesized by the microwave-assisted technique crystallize in the form of thin hexagonal plates aggregated into spheroidal particles. Depending on the conditions of microwave-assisted hydrothermal synthesis, the formation of several phases differing in interplanar spacing along the [00l] direction is possible. The materials obtained are shown to possess good anion-exchange properties. This work provides a route to large-scale synthesis of LRH-based advanced materials. This journal is

    Original languageEnglish
    Pages (from-to)2667-2674
    Number of pages8
    JournalCrystEngComm
    Volume17
    Issue number13
    DOIs
    Publication statusPublished - 7 Apr 2015

    Fingerprint

    Microwaves
    microwaves
    synthesis
    Rare earth compounds
    Yttrium
    rare earth compounds
    Hydrothermal synthesis
    yttrium
    Anions
    Ion exchange
    Negative ions
    routes
    spacing
    anions
    Direction compound

    ASJC Scopus subject areas

    • Chemistry(all)
    • Materials Science(all)
    • Condensed Matter Physics

    Cite this

    Yapryntsev, A. D., Baranchikov, A. E., Skogareva, L. S., Goldt, A. E., Stolyarov, I. P., Ivanova, O. S., ... Ivanov, V. K. (2015). High-yield microwave synthesis of layered Y2(OH)5NO3·xH2O materials. CrystEngComm, 17(13), 2667-2674. https://doi.org/10.1039/c4ce02303j

    High-yield microwave synthesis of layered Y2(OH)5NO3·xH2O materials. / Yapryntsev, A. D.; Baranchikov, A. E.; Skogareva, L. S.; Goldt, A. E.; Stolyarov, I. P.; Ivanova, O. S.; Kozik, V. V.; Ivanov, V. K.

    In: CrystEngComm, Vol. 17, No. 13, 07.04.2015, p. 2667-2674.

    Research output: Contribution to journalArticle

    Yapryntsev, AD, Baranchikov, AE, Skogareva, LS, Goldt, AE, Stolyarov, IP, Ivanova, OS, Kozik, VV & Ivanov, VK 2015, 'High-yield microwave synthesis of layered Y2(OH)5NO3·xH2O materials', CrystEngComm, vol. 17, no. 13, pp. 2667-2674. https://doi.org/10.1039/c4ce02303j
    Yapryntsev AD, Baranchikov AE, Skogareva LS, Goldt AE, Stolyarov IP, Ivanova OS et al. High-yield microwave synthesis of layered Y2(OH)5NO3·xH2O materials. CrystEngComm. 2015 Apr 7;17(13):2667-2674. https://doi.org/10.1039/c4ce02303j
    Yapryntsev, A. D. ; Baranchikov, A. E. ; Skogareva, L. S. ; Goldt, A. E. ; Stolyarov, I. P. ; Ivanova, O. S. ; Kozik, V. V. ; Ivanov, V. K. / High-yield microwave synthesis of layered Y2(OH)5NO3·xH2O materials. In: CrystEngComm. 2015 ; Vol. 17, No. 13. pp. 2667-2674.
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