Formation and properties of micro-arc wollastonite-calcium phosphate coatings on titanium and zirconium-niobium alloy

M. B. Sedelnikova, E. G. Komarova, Yu P. Sharkeev, A. A. Shinzhina

Research School of High-Energy Physics

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Abstract

Wollastonite-calcium phosphate (W-CaP) coatings were deposited by the micro-arc oxidation (MAO) method on titanium (Ti) and Zr-1 wt % Nb (Zr-1Nb) alloy. The voltage of 150-300 V generated the MAO process with initial current amplitudes of 150-550 A and 100-350 A for Ti and Zr-1Nb substrates, respectively. Thin W-CaP coatings with the thickness of 10-11 μm were formed on Ti and Zr-1Nb under the low process voltage of 130-150 V. Elongated wollastonite particles with the size in the range of 40-100 μm were observed in such coatings. The structure of the coatings on Ti was mainly in X-ray amorphous state. In this case, X-ray reflexes relating to the crystalline phases of Ti and wollastonite were observed only in XRD patterns of the coatings deposited under 150-200 V. While, the crystalline structure with phases of CaZr₄(PO₄)₆, β-ZrP₂O₇, ZrO₂, and Zr was detected in the coatings on Zr-1Nb. FT-IRS, XRD, and SEM data confirmed that the increase of the process voltage up to 300 V leads to the dissociation of the wollastonite.

Original language	English
Title of host publication	Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016: Proceedings of the International Conference on Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016
Subtitle of host publication	Proceedings of the International Conference on Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016
Publisher	American Institute of Physics Inc.
Volume	1783
ISBN (Electronic)	9780735414457
DOIs	https://doi.org/10.1063/1.4966496
Publication status	Published - 10 Nov 2016
Event	International Conference on Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016 - Tomsk, Russian Federation Duration: 19 Sep 2016 → 23 Sep 2016

Conference

Conference	International Conference on Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016
Country	Russian Federation
City	Tomsk
Period	19.9.16 → 23.9.16

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ASJC Scopus subject areas

Physics and Astronomy(all)

Cite this

Sedelnikova, M. B., Komarova, E. G., Sharkeev, Y. P., & Shinzhina, A. A. (2016). Formation and properties of micro-arc wollastonite-calcium phosphate coatings on titanium and zirconium-niobium alloy. In Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016: Proceedings of the International Conference on Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016: Proceedings of the International Conference on Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016 (Vol. 1783). [020202] American Institute of Physics Inc.. https://doi.org/10.1063/1.4966496

Formation and properties of micro-arc wollastonite-calcium phosphate coatings on titanium and zirconium-niobium alloy. / Sedelnikova, M. B.; Komarova, E. G.; Sharkeev, Yu P.; Shinzhina, A. A.

Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016: Proceedings of the International Conference on Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016: Proceedings of the International Conference on Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016. Vol. 1783 American Institute of Physics Inc., 2016. 020202.

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Sedelnikova, MB, Komarova, EG, Sharkeev, YP & Shinzhina, AA 2016, Formation and properties of micro-arc wollastonite-calcium phosphate coatings on titanium and zirconium-niobium alloy. in Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016: Proceedings of the International Conference on Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016: Proceedings of the International Conference on Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016. vol. 1783, 020202, American Institute of Physics Inc., International Conference on Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016, Tomsk, Russian Federation, 19.9.16. https://doi.org/10.1063/1.4966496

Sedelnikova MB, Komarova EG, Sharkeev YP, Shinzhina AA. Formation and properties of micro-arc wollastonite-calcium phosphate coatings on titanium and zirconium-niobium alloy. In Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016: Proceedings of the International Conference on Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016: Proceedings of the International Conference on Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016. Vol. 1783. American Institute of Physics Inc. 2016. 020202 https://doi.org/10.1063/1.4966496

Sedelnikova, M. B. ; Komarova, E. G. ; Sharkeev, Yu P. ; Shinzhina, A. A. / Formation and properties of micro-arc wollastonite-calcium phosphate coatings on titanium and zirconium-niobium alloy. Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016: Proceedings of the International Conference on Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016: Proceedings of the International Conference on Advanced Materials with Hierarchical Structure for New Technologies and Reliable Structures 2016. Vol. 1783 American Institute of Physics Inc., 2016.

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abstract = "Wollastonite-calcium phosphate (W-CaP) coatings were deposited by the micro-arc oxidation (MAO) method on titanium (Ti) and Zr-1 wt {\%} Nb (Zr-1Nb) alloy. The voltage of 150-300 V generated the MAO process with initial current amplitudes of 150-550 A and 100-350 A for Ti and Zr-1Nb substrates, respectively. Thin W-CaP coatings with the thickness of 10-11 μm were formed on Ti and Zr-1Nb under the low process voltage of 130-150 V. Elongated wollastonite particles with the size in the range of 40-100 μm were observed in such coatings. The structure of the coatings on Ti was mainly in X-ray amorphous state. In this case, X-ray reflexes relating to the crystalline phases of Ti and wollastonite were observed only in XRD patterns of the coatings deposited under 150-200 V. While, the crystalline structure with phases of CaZr4(PO4)6, β-ZrP2O7, ZrO2, and Zr was detected in the coatings on Zr-1Nb. FT-IRS, XRD, and SEM data confirmed that the increase of the process voltage up to 300 V leads to the dissociation of the wollastonite.",

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Access to Document

10.1063/1.4966496