Estimation of thermomagnetometry method sensitivity for magnetic phase determination

Abstract

In this article, the sensitivity of thermomagnetometry method for magnetic phase determination in lithium substituted ferrites was estimated by thermogravimetric analysis in magnetic field of lithium-zinc ferrite and iron dioxide (Li_0.4Fe_2.4Zn_0.2O₄+α-Fe₂O₃) components mixture with different mass proportions: 2, 4, 6, and 100 mass% Li_0.4Fe_2.4Zn_0.2O₄ phase in total mixture. Thereby, analyzed samples are mixture of magnetic and nonmagnetic phases. Results of thermomagnetometric analysis were supplemented with the X-Ray diffraction analysis data. It was shown that the thermomagnetometry method allows to determine a magnetic phases with mass content not less than 2 mass% in analyzed mixture. In this case, we can clearly estimate the position and intensity of the peak on derivative thermogravimetric curve, which connected with a magnetic phase transition in ferrite at Curie temperature.

Original language	English
Article number	012090
Journal	IOP Conference Series: Materials Science and Engineering
Volume	110
Issue number	1
DOIs	https://doi.org/10.1088/1757-899X/110/1/012090
Publication status	Published - 23 Feb 2016
Event	11th International Scientific Conference on Radiation-Thermal Effects and Processes in Inorganic Materials 2015, RTEP 2015 - Tomsk, Russian Federation Duration: 31 Aug 2015 → 10 Sep 2015

Keywords

ferrospinel
lithium-substituted ferrospinel
lithium-zinc ferrite
thermomagnetometry method
X-Ray analysis

ASJC Scopus subject areas

Materials Science(all)
Engineering(all)

Access to Document

10.1088/1757-899X/110/1/012090

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@article{453f0ae112b94f76afc9b1ae65a8bc91,

title = "Estimation of thermomagnetometry method sensitivity for magnetic phase determination",

abstract = "In this article, the sensitivity of thermomagnetometry method for magnetic phase determination in lithium substituted ferrites was estimated by thermogravimetric analysis in magnetic field of lithium-zinc ferrite and iron dioxide (Li0.4Fe2.4Zn0.2O4+α-Fe2O3) components mixture with different mass proportions: 2, 4, 6, and 100 mass% Li0.4Fe2.4Zn0.2O4 phase in total mixture. Thereby, analyzed samples are mixture of magnetic and nonmagnetic phases. Results of thermomagnetometric analysis were supplemented with the X-Ray diffraction analysis data. It was shown that the thermomagnetometry method allows to determine a magnetic phases with mass content not less than 2 mass% in analyzed mixture. In this case, we can clearly estimate the position and intensity of the peak on derivative thermogravimetric curve, which connected with a magnetic phase transition in ferrite at Curie temperature.",

keywords = "ferrospinel, lithium-substituted ferrospinel, lithium-zinc ferrite, thermomagnetometry method, X-Ray analysis",

author = "Astafyev, {A. L.} and Surzhikov, {Anatoly Petrovich} and Lysenko, {E. N.}",

year = "2016",

month = feb,

day = "23",

doi = "10.1088/1757-899X/110/1/012090",

language = "English",

volume = "110",

journal = "IOP Conference Series: Materials Science and Engineering",

issn = "1757-8981",

publisher = "IOP Publishing Ltd.",

number = "1",

note = "11th International Scientific Conference on Radiation-Thermal Effects and Processes in Inorganic Materials 2015, RTEP 2015 ; Conference date: 31-08-2015 Through 10-09-2015",

}

TY - JOUR

T1 - Estimation of thermomagnetometry method sensitivity for magnetic phase determination

AU - Astafyev, A. L.

AU - Surzhikov, Anatoly Petrovich

AU - Lysenko, E. N.

PY - 2016/2/23

Y1 - 2016/2/23

N2 - In this article, the sensitivity of thermomagnetometry method for magnetic phase determination in lithium substituted ferrites was estimated by thermogravimetric analysis in magnetic field of lithium-zinc ferrite and iron dioxide (Li0.4Fe2.4Zn0.2O4+α-Fe2O3) components mixture with different mass proportions: 2, 4, 6, and 100 mass% Li0.4Fe2.4Zn0.2O4 phase in total mixture. Thereby, analyzed samples are mixture of magnetic and nonmagnetic phases. Results of thermomagnetometric analysis were supplemented with the X-Ray diffraction analysis data. It was shown that the thermomagnetometry method allows to determine a magnetic phases with mass content not less than 2 mass% in analyzed mixture. In this case, we can clearly estimate the position and intensity of the peak on derivative thermogravimetric curve, which connected with a magnetic phase transition in ferrite at Curie temperature.

AB - In this article, the sensitivity of thermomagnetometry method for magnetic phase determination in lithium substituted ferrites was estimated by thermogravimetric analysis in magnetic field of lithium-zinc ferrite and iron dioxide (Li0.4Fe2.4Zn0.2O4+α-Fe2O3) components mixture with different mass proportions: 2, 4, 6, and 100 mass% Li0.4Fe2.4Zn0.2O4 phase in total mixture. Thereby, analyzed samples are mixture of magnetic and nonmagnetic phases. Results of thermomagnetometric analysis were supplemented with the X-Ray diffraction analysis data. It was shown that the thermomagnetometry method allows to determine a magnetic phases with mass content not less than 2 mass% in analyzed mixture. In this case, we can clearly estimate the position and intensity of the peak on derivative thermogravimetric curve, which connected with a magnetic phase transition in ferrite at Curie temperature.

KW - ferrospinel

KW - lithium-substituted ferrospinel

KW - lithium-zinc ferrite

KW - thermomagnetometry method

KW - X-Ray analysis

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U2 - 10.1088/1757-899X/110/1/012090

DO - 10.1088/1757-899X/110/1/012090

M3 - Conference article

AN - SCOPUS:84971634593

VL - 110

JO - IOP Conference Series: Materials Science and Engineering

JF - IOP Conference Series: Materials Science and Engineering

SN - 1757-8981

IS - 1

M1 - 012090

T2 - 11th International Scientific Conference on Radiation-Thermal Effects and Processes in Inorganic Materials 2015, RTEP 2015

Y2 - 31 August 2015 through 10 September 2015