Effect of ultrasonic surface treatment of steel 40Kh13 on the microstructure of nitrided layer formed by high-intensity low-energy implantation with nitrogen ions

V. A. Klimenov, Zh G. Kovalevskaya, O. B. Perevalova, Yu F. Ivanov, V. A. Kukareko

Research output: Contribution to journalArticle

2 Citations (Scopus)

Abstract

X-ray diffraction and transmission electron microscopy were used to study the microstructure and phase composition of surface layers of steel 40Kh13 subjected to irradiation with high-intensity low-energy ion beams, ultrasonic surface modification, and combined treatment including ultrasonic surface modification and ion implantation. It was found that the ultrasonic modification of steel surface leads to changes in the structure of tempered martensite and the formation of grain structure with a grain size of 0.3 μm and nanosized special carbides Cr23C6 in the martensite lamellae. The ion implantation into this steel results in the formation of a nitrided layer consisting of a nitride region, which represents a mixture of several phases (α-, γ-, ε, and ultrafine chromium nitrides), and a zone of internal nitriding (α″ and nitrogen-containing martensite αN). The preliminary ultrasonic modification causes an increase in the nanohardness and in the thickness of the nitrided layer, which is due to the more intense penetration of nitrogen atoms into the surface layer and an increase in the volume fraction of iron nitrides and density of ultrafine chromium nitrides in this layer.

Original languageEnglish
Pages (from-to)578-586
Number of pages9
JournalPhysics of Metals and Metallography
Volume102
Issue number6
DOIs
Publication statusPublished - Dec 2006

Fingerprint

nitrogen ions
Steel
surface treatment
Nitrides
Ion implantation
nitrides
Surface treatment
implantation
Nitrogen
ultrasonics
Ultrasonics
martensite
Martensite
steels
Ions
microstructure
Microstructure
Chromium
ion implantation
chromium

ASJC Scopus subject areas

  • Metals and Alloys

Cite this

@article{a486cac0e47c46cf8176d6fd5a588568,
title = "Effect of ultrasonic surface treatment of steel 40Kh13 on the microstructure of nitrided layer formed by high-intensity low-energy implantation with nitrogen ions",
abstract = "X-ray diffraction and transmission electron microscopy were used to study the microstructure and phase composition of surface layers of steel 40Kh13 subjected to irradiation with high-intensity low-energy ion beams, ultrasonic surface modification, and combined treatment including ultrasonic surface modification and ion implantation. It was found that the ultrasonic modification of steel surface leads to changes in the structure of tempered martensite and the formation of grain structure with a grain size of 0.3 μm and nanosized special carbides Cr23C6 in the martensite lamellae. The ion implantation into this steel results in the formation of a nitrided layer consisting of a nitride region, which represents a mixture of several phases (α-, γ-, ε, and ultrafine chromium nitrides), and a zone of internal nitriding (α″ and nitrogen-containing martensite αN). The preliminary ultrasonic modification causes an increase in the nanohardness and in the thickness of the nitrided layer, which is due to the more intense penetration of nitrogen atoms into the surface layer and an increase in the volume fraction of iron nitrides and density of ultrafine chromium nitrides in this layer.",
author = "Klimenov, {V. A.} and Kovalevskaya, {Zh G.} and Perevalova, {O. B.} and Ivanov, {Yu F.} and Kukareko, {V. A.}",
year = "2006",
month = "12",
doi = "10.1134/S0031918X06120040",
language = "English",
volume = "102",
pages = "578--586",
journal = "Physics of Metals and Metallography",
issn = "0031-918X",
publisher = "Maik Nauka-Interperiodica Publishing",
number = "6",

}

TY - JOUR

T1 - Effect of ultrasonic surface treatment of steel 40Kh13 on the microstructure of nitrided layer formed by high-intensity low-energy implantation with nitrogen ions

AU - Klimenov, V. A.

AU - Kovalevskaya, Zh G.

AU - Perevalova, O. B.

AU - Ivanov, Yu F.

AU - Kukareko, V. A.

PY - 2006/12

Y1 - 2006/12

N2 - X-ray diffraction and transmission electron microscopy were used to study the microstructure and phase composition of surface layers of steel 40Kh13 subjected to irradiation with high-intensity low-energy ion beams, ultrasonic surface modification, and combined treatment including ultrasonic surface modification and ion implantation. It was found that the ultrasonic modification of steel surface leads to changes in the structure of tempered martensite and the formation of grain structure with a grain size of 0.3 μm and nanosized special carbides Cr23C6 in the martensite lamellae. The ion implantation into this steel results in the formation of a nitrided layer consisting of a nitride region, which represents a mixture of several phases (α-, γ-, ε, and ultrafine chromium nitrides), and a zone of internal nitriding (α″ and nitrogen-containing martensite αN). The preliminary ultrasonic modification causes an increase in the nanohardness and in the thickness of the nitrided layer, which is due to the more intense penetration of nitrogen atoms into the surface layer and an increase in the volume fraction of iron nitrides and density of ultrafine chromium nitrides in this layer.

AB - X-ray diffraction and transmission electron microscopy were used to study the microstructure and phase composition of surface layers of steel 40Kh13 subjected to irradiation with high-intensity low-energy ion beams, ultrasonic surface modification, and combined treatment including ultrasonic surface modification and ion implantation. It was found that the ultrasonic modification of steel surface leads to changes in the structure of tempered martensite and the formation of grain structure with a grain size of 0.3 μm and nanosized special carbides Cr23C6 in the martensite lamellae. The ion implantation into this steel results in the formation of a nitrided layer consisting of a nitride region, which represents a mixture of several phases (α-, γ-, ε, and ultrafine chromium nitrides), and a zone of internal nitriding (α″ and nitrogen-containing martensite αN). The preliminary ultrasonic modification causes an increase in the nanohardness and in the thickness of the nitrided layer, which is due to the more intense penetration of nitrogen atoms into the surface layer and an increase in the volume fraction of iron nitrides and density of ultrafine chromium nitrides in this layer.

UR - http://www.scopus.com/inward/record.url?scp=33845607146&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=33845607146&partnerID=8YFLogxK

U2 - 10.1134/S0031918X06120040

DO - 10.1134/S0031918X06120040

M3 - Article

VL - 102

SP - 578

EP - 586

JO - Physics of Metals and Metallography

JF - Physics of Metals and Metallography

SN - 0031-918X

IS - 6

ER -