Effect of pulsed electron beam treatment on the physico-mechanical properties of hydroxyapatite-coated titanium

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Abstract

The effect of the pulsed electron beam (PEB) treatment on the structure and morphology of the hydroxyapatite (HA) coating deposited on the surfaces of titanium substrates by radio frequency magnetron sputtering was elucidated. The structure, composition and morphology of the samples were characterized by scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS) and X-ray diffraction (XRD). The results collected from SEM experiments demonstrated that the HA film was smooth and featureless. The samples were irradiated by PEB using an electron beam energy density of 0.1 J cm-2, electron beam pulse duration of 50 μs, pulse repetition frequency of 5 Hz, and number of pulses N=50 and N=150. After PEB treatment with N=50, the coating exhibited a much finer uniform surface morphology, playing a crucial role in the enhancement of the mechanical properties of the HA-coated titanium substrate. The surface of the HA film treated with N=150 was still smooth and featureless. The XRD data demonstrated that PEB treatment of HA films produced only a slight decrease in the HA phase content. The combination of these two techniques opens the possibility of preparing high quality HA layers.

Original languageEnglish
Pages (from-to)1470-1475
Number of pages6
JournalCeramics International
Volume42
Issue number1
DOIs
Publication statusPublished - 1 Jan 2016

Fingerprint

Durapatite
Titanium
Hydroxyapatite
Electron beams
Mechanical properties
X ray diffraction
Coatings
Scanning electron microscopy
Substrates
Magnetron sputtering
Surface morphology
X ray photoelectron spectroscopy
Chemical analysis
Experiments

Keywords

  • Acid etching
  • Calcium phosphate
  • Hydroxyapatite coating
  • Pulsed electron beam treatment
  • RF-magnetron sputtering

ASJC Scopus subject areas

  • Ceramics and Composites
  • Process Chemistry and Technology
  • Electronic, Optical and Magnetic Materials
  • Surfaces, Coatings and Films
  • Materials Chemistry

Cite this

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title = "Effect of pulsed electron beam treatment on the physico-mechanical properties of hydroxyapatite-coated titanium",
abstract = "The effect of the pulsed electron beam (PEB) treatment on the structure and morphology of the hydroxyapatite (HA) coating deposited on the surfaces of titanium substrates by radio frequency magnetron sputtering was elucidated. The structure, composition and morphology of the samples were characterized by scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS) and X-ray diffraction (XRD). The results collected from SEM experiments demonstrated that the HA film was smooth and featureless. The samples were irradiated by PEB using an electron beam energy density of 0.1 J cm-2, electron beam pulse duration of 50 μs, pulse repetition frequency of 5 Hz, and number of pulses N=50 and N=150. After PEB treatment with N=50, the coating exhibited a much finer uniform surface morphology, playing a crucial role in the enhancement of the mechanical properties of the HA-coated titanium substrate. The surface of the HA film treated with N=150 was still smooth and featureless. The XRD data demonstrated that PEB treatment of HA films produced only a slight decrease in the HA phase content. The combination of these two techniques opens the possibility of preparing high quality HA layers.",
keywords = "Acid etching, Calcium phosphate, Hydroxyapatite coating, Pulsed electron beam treatment, RF-magnetron sputtering",
author = "Surmeneva, {M. A.} and Chudinova, {E. A.} and Grubova, {I. Yu} and Korneva, {Olga Sergeevna} and Shulepov, {I. A.} and Teresov, {A. D.} and Koval, {Nikolay Nikolaevich} and J. Mayer and C. Oehr and Surmenev, {R. A.}",
year = "2016",
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T1 - Effect of pulsed electron beam treatment on the physico-mechanical properties of hydroxyapatite-coated titanium

AU - Surmeneva, M. A.

AU - Chudinova, E. A.

AU - Grubova, I. Yu

AU - Korneva, Olga Sergeevna

AU - Shulepov, I. A.

AU - Teresov, A. D.

AU - Koval, Nikolay Nikolaevich

AU - Mayer, J.

AU - Oehr, C.

AU - Surmenev, R. A.

PY - 2016/1/1

Y1 - 2016/1/1

N2 - The effect of the pulsed electron beam (PEB) treatment on the structure and morphology of the hydroxyapatite (HA) coating deposited on the surfaces of titanium substrates by radio frequency magnetron sputtering was elucidated. The structure, composition and morphology of the samples were characterized by scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS) and X-ray diffraction (XRD). The results collected from SEM experiments demonstrated that the HA film was smooth and featureless. The samples were irradiated by PEB using an electron beam energy density of 0.1 J cm-2, electron beam pulse duration of 50 μs, pulse repetition frequency of 5 Hz, and number of pulses N=50 and N=150. After PEB treatment with N=50, the coating exhibited a much finer uniform surface morphology, playing a crucial role in the enhancement of the mechanical properties of the HA-coated titanium substrate. The surface of the HA film treated with N=150 was still smooth and featureless. The XRD data demonstrated that PEB treatment of HA films produced only a slight decrease in the HA phase content. The combination of these two techniques opens the possibility of preparing high quality HA layers.

AB - The effect of the pulsed electron beam (PEB) treatment on the structure and morphology of the hydroxyapatite (HA) coating deposited on the surfaces of titanium substrates by radio frequency magnetron sputtering was elucidated. The structure, composition and morphology of the samples were characterized by scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS) and X-ray diffraction (XRD). The results collected from SEM experiments demonstrated that the HA film was smooth and featureless. The samples were irradiated by PEB using an electron beam energy density of 0.1 J cm-2, electron beam pulse duration of 50 μs, pulse repetition frequency of 5 Hz, and number of pulses N=50 and N=150. After PEB treatment with N=50, the coating exhibited a much finer uniform surface morphology, playing a crucial role in the enhancement of the mechanical properties of the HA-coated titanium substrate. The surface of the HA film treated with N=150 was still smooth and featureless. The XRD data demonstrated that PEB treatment of HA films produced only a slight decrease in the HA phase content. The combination of these two techniques opens the possibility of preparing high quality HA layers.

KW - Acid etching

KW - Calcium phosphate

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KW - RF-magnetron sputtering

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