Effect of citric acid and ethylene glycol on the formation of calcium aluminate via the sol-gel method

Abstract

The processes of formation of calcium aluminate via the sol-gel method has been studied by IR spectroscopy, thermal analysis, X-ray powder diffraction, and scanning electron microscopy. The key stages of synthesis to obtain orthorhombic calcium aluminate (solvent removal, stepwise decomposition of the organic polymeric framework, and formation of crystalline aluminate) have been determined. The effect of the composition of the starting mixture on the formation process and the surface morphology of the final product has been demonstrated.

Original language	English
Pages (from-to)	450-455
Number of pages	6
Journal	Russian Journal of Inorganic Chemistry
Volume	58
Issue number	4
DOIs	https://doi.org/10.1134/S0036023613040165
Publication status	Published - Apr 2013

ASJC Scopus subject areas

Inorganic Chemistry

Access to Document

10.1134/S0036023613040165

Fingerprint Dive into the research topics of 'Effect of citric acid and ethylene glycol on the formation of calcium aluminate via the sol-gel method'. Together they form a unique fingerprint.

Cite this

@article{a2f8e95f822d44f28f939ade5ad0163e,

title = "Effect of citric acid and ethylene glycol on the formation of calcium aluminate via the sol-gel method",

abstract = "The processes of formation of calcium aluminate via the sol-gel method has been studied by IR spectroscopy, thermal analysis, X-ray powder diffraction, and scanning electron microscopy. The key stages of synthesis to obtain orthorhombic calcium aluminate (solvent removal, stepwise decomposition of the organic polymeric framework, and formation of crystalline aluminate) have been determined. The effect of the composition of the starting mixture on the formation process and the surface morphology of the final product has been demonstrated.",

author = "Selyunina, {L. A.} and Mishenina, {L. N.} and Slizhov, {Yu G.} and Kozik, {V. V.}",

year = "2013",

month = apr,

doi = "10.1134/S0036023613040165",

language = "English",

volume = "58",

pages = "450--455",

journal = "Russian Journal of Inorganic Chemistry",

issn = "0036-0236",

publisher = "Maik Nauka-Interperiodica Publishing",

number = "4",

}

TY - JOUR

T1 - Effect of citric acid and ethylene glycol on the formation of calcium aluminate via the sol-gel method

AU - Selyunina, L. A.

AU - Mishenina, L. N.

AU - Slizhov, Yu G.

AU - Kozik, V. V.

PY - 2013/4

Y1 - 2013/4

N2 - The processes of formation of calcium aluminate via the sol-gel method has been studied by IR spectroscopy, thermal analysis, X-ray powder diffraction, and scanning electron microscopy. The key stages of synthesis to obtain orthorhombic calcium aluminate (solvent removal, stepwise decomposition of the organic polymeric framework, and formation of crystalline aluminate) have been determined. The effect of the composition of the starting mixture on the formation process and the surface morphology of the final product has been demonstrated.

AB - The processes of formation of calcium aluminate via the sol-gel method has been studied by IR spectroscopy, thermal analysis, X-ray powder diffraction, and scanning electron microscopy. The key stages of synthesis to obtain orthorhombic calcium aluminate (solvent removal, stepwise decomposition of the organic polymeric framework, and formation of crystalline aluminate) have been determined. The effect of the composition of the starting mixture on the formation process and the surface morphology of the final product has been demonstrated.

UR - http://www.scopus.com/inward/record.url?scp=84879873290&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=84879873290&partnerID=8YFLogxK

U2 - 10.1134/S0036023613040165

DO - 10.1134/S0036023613040165

M3 - Article

AN - SCOPUS:84879873290

VL - 58

SP - 450

EP - 455

JO - Russian Journal of Inorganic Chemistry

JF - Russian Journal of Inorganic Chemistry

SN - 0036-0236

IS - 4

ER -