Abstract
The reagent obtained from iodine monochloride and silver sulfate in sulfuric acid easily iodinates 1-methyl-3-nitropyrazole under mild conditions to give 4-iodo or 4,5-diiodo derivatives. 1-Methyl-4-nitropyrazole was also directly iodinated with this reagent for the first time.
| Original language | English |
|---|---|
| Pages (from-to) | 1475-1477 |
| Number of pages | 3 |
| Journal | Russian Chemical Bulletin |
| Volume | 49 |
| Issue number | 8 |
| DOIs | |
| Publication status | Published - 1 Jan 2000 |
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Keywords
- Iodination
- Iodine monochloride
- Iodomethylnitro-pyrazoles
- Methylnitropyrazoles
ASJC Scopus subject areas
- Chemistry(all)
Cite this
Direct iodination of 3- and 4-nitropyrazoles with a reagent based on iodine monochloride and silver sulfate. / Chaikovskii, V. K.; Kharlova, T. S.; Tretyakov, E. V.; Vasilevsky, S. F.; Filimonov, V. D.
In: Russian Chemical Bulletin, Vol. 49, No. 8, 01.01.2000, p. 1475-1477.Research output: Contribution to journal › Article
}
TY - JOUR
T1 - Direct iodination of 3- and 4-nitropyrazoles with a reagent based on iodine monochloride and silver sulfate
AU - Chaikovskii, V. K.
AU - Kharlova, T. S.
AU - Tretyakov, E. V.
AU - Vasilevsky, S. F.
AU - Filimonov, V. D.
PY - 2000/1/1
Y1 - 2000/1/1
N2 - The reagent obtained from iodine monochloride and silver sulfate in sulfuric acid easily iodinates 1-methyl-3-nitropyrazole under mild conditions to give 4-iodo or 4,5-diiodo derivatives. 1-Methyl-4-nitropyrazole was also directly iodinated with this reagent for the first time.
AB - The reagent obtained from iodine monochloride and silver sulfate in sulfuric acid easily iodinates 1-methyl-3-nitropyrazole under mild conditions to give 4-iodo or 4,5-diiodo derivatives. 1-Methyl-4-nitropyrazole was also directly iodinated with this reagent for the first time.
KW - Iodination
KW - Iodine monochloride
KW - Iodomethylnitro-pyrazoles
KW - Methylnitropyrazoles
UR - http://www.scopus.com/inward/record.url?scp=0034342728&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=0034342728&partnerID=8YFLogxK
U2 - 10.1007/BF02495102
DO - 10.1007/BF02495102
M3 - Article
VL - 49
SP - 1475
EP - 1477
JO - Russian Chemical Bulletin
JF - Russian Chemical Bulletin
SN - 0568-5230
IS - 8
ER -