Development of control method for ferrite phase composition using thermomagnetometric analysis

Research output: Chapter in Book/Report/Conference proceedingConference contribution

5 Citations (Scopus)

Abstract

In this paper we evaluated the phase composition of products in synthesis of Li 0.4Fe 2.4Zn 0.2O 4 and Li 0.3Fe 2.3Zn 0.4O 4 lithium-substituted ferrites using thermomagnetometric method. Results of thermomagnetometric analysis were compared with X-ray diffraction (XRD) data. It was found that thermomagnetometric analysis in comparison with XRD method better reflects the temperature of phase magnetic transitions and therefore provides a more precise estimate the phase composition of the samples. However, a complex analysis using of both X-ray and thermomagnetometry methods will be the most optimal in case of the formation of non-magnetic or weakly magnetic phases. By the thermomagnetometric analysis it was shown that the homogeneity of synthesized under the same temperature-time regimes ferrites decreases with increasing the concentration of zinc in the initial mixture. Using of intermediate grinding and mixing leads to homogeneity increasing of synthesized ferrite with higher content of the final phase.

Original languageEnglish
Title of host publicationIOP Conference Series: Materials Science and Engineering
PublisherInstitute of Physics Publishing
Volume66
Edition1
DOIs
Publication statusPublished - 2014
Event20th International Conference for Students and Young Scientists: Modern Techniques and Technologies, MTT 2014 - Tomsk, Russian Federation
Duration: 14 Apr 201418 Apr 2014

Other

Other20th International Conference for Students and Young Scientists: Modern Techniques and Technologies, MTT 2014
CountryRussian Federation
CityTomsk
Period14.4.1418.4.14

Keywords

  • Ferrite
  • Lithium-substituted ferrospinels
  • Thermomagnetometry method
  • X-ray diffraction

ASJC Scopus subject areas

  • Engineering(all)
  • Materials Science(all)

Fingerprint Dive into the research topics of 'Development of control method for ferrite phase composition using thermomagnetometric analysis'. Together they form a unique fingerprint.

Cite this