Abstract
Optimum conditions are described for HPLC determination of 1-hydroxypyrene with electrochemical detection (ED) giving the detection limit ∼ 1.10-8 mol.l-1. This detection limit was compared with that for UV spectrophotometric detection (∼ 1.10-7 mol.l-1) and fluorimetric detection (∼ 5.10-10 mol.l-1). It was demonstrated that HPLC-ED can be used for the determination of 1-hydroxypyrene in urine down to 1.10-7 mol.l-1 and thus for biological monitoring of human exposure to polycyclic aromatic hydrocarbons.
| Original language | English |
|---|---|
| Pages (from-to) | 875-876 |
| Number of pages | 2 |
| Journal | Chemicke Listy |
| Volume | 91 |
| Issue number | 10 |
| Publication status | Published - 1 Dec 1997 |
| Externally published | Yes |
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ASJC Scopus subject areas
- Chemistry(all)
Cite this
Determination of 1-Hydroxypyrene Using High-Performance Liquid Chromatography with Electrochemical Detection. / Barek, J.; Bencko, V.; Cvačka, J.; Mejstřík, V.; Slámová, A.; Švagrová, I.; Zima, J.
In: Chemicke Listy, Vol. 91, No. 10, 01.12.1997, p. 875-876.Research output: Contribution to journal › Article
}
TY - JOUR
T1 - Determination of 1-Hydroxypyrene Using High-Performance Liquid Chromatography with Electrochemical Detection
AU - Barek, J.
AU - Bencko, V.
AU - Cvačka, J.
AU - Mejstřík, V.
AU - Slámová, A.
AU - Švagrová, I.
AU - Zima, J.
PY - 1997/12/1
Y1 - 1997/12/1
N2 - Optimum conditions are described for HPLC determination of 1-hydroxypyrene with electrochemical detection (ED) giving the detection limit ∼ 1.10-8 mol.l-1. This detection limit was compared with that for UV spectrophotometric detection (∼ 1.10-7 mol.l-1) and fluorimetric detection (∼ 5.10-10 mol.l-1). It was demonstrated that HPLC-ED can be used for the determination of 1-hydroxypyrene in urine down to 1.10-7 mol.l-1 and thus for biological monitoring of human exposure to polycyclic aromatic hydrocarbons.
AB - Optimum conditions are described for HPLC determination of 1-hydroxypyrene with electrochemical detection (ED) giving the detection limit ∼ 1.10-8 mol.l-1. This detection limit was compared with that for UV spectrophotometric detection (∼ 1.10-7 mol.l-1) and fluorimetric detection (∼ 5.10-10 mol.l-1). It was demonstrated that HPLC-ED can be used for the determination of 1-hydroxypyrene in urine down to 1.10-7 mol.l-1 and thus for biological monitoring of human exposure to polycyclic aromatic hydrocarbons.
UR - http://www.scopus.com/inward/record.url?scp=0347170810&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=0347170810&partnerID=8YFLogxK
M3 - Article
AN - SCOPUS:0347170810
VL - 91
SP - 875
EP - 876
JO - Chemicke Listy
JF - Chemicke Listy
SN - 0009-2770
IS - 10
ER -