Deposition of calcium phosphate coatings using radio frequency magnetron sputtering of substituted β-tricalcium phosphate targets

A. Y. Fedotkin, E. N. Bolbasov, A. I. Kozelskaya, A. S. Useinov, S. I. Tverdokhlebov

Research output: Contribution to journalConference article

Abstract

The influence of magnesium and/or strontium substitutions on the deposition rate of P-TCP was investigated. Pure β-TCP, Mg-β-TCP, Sr-β-TCP and Mg/Sr-β-TCP targets were used for the coating formation. It was shown that strontium substitutions in the structure of β-TCP target increase the deposition rate of coatings. Magnesium substitutions, on the contrary, decrease this parameter. It makes it possible to increase the deposition rate of coatings formed by radio frequency magnetron sputtering without any negative effect on coatings properties. It was demonstrated that all coatings formed by radio frequency magnetron sputtering of β-TCP targets were calcium-rich. The methods of AFM and SEM revealed that coatings under study were characterized by various morphologies. Magnesium-containing coatings (Mg-β-TCP and Mg/Sr-β-TCP) had the lower value of nanohardness than other ones. All coatings were characterized by the higher value of surface free energy than titanium substrate. The coatings formed by sputtering of β-TCP, Mg-β-TCP, Sr-β-TCP had approximately the same value of this parameter.

Original languageEnglish
Article number032070
JournalJournal of Physics: Conference Series
Volume1115
Issue number3
DOIs
Publication statusPublished - 27 Nov 2018
Event6th International Congress on Energy Fluxes and Radiation Effects 2018, EFRE 2018 - Tomsk, Russian Federation
Duration: 16 Sep 201822 Sep 2018

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calcium phosphates
radio frequencies
magnetron sputtering
phosphates
coatings
magnesium
substitutes
strontium
calcium
titanium
sputtering
free energy
atomic force microscopy
scanning electron microscopy

ASJC Scopus subject areas

  • Physics and Astronomy(all)

Cite this

@article{b006555c14d446e3ab9ebcfdc782121c,
title = "Deposition of calcium phosphate coatings using radio frequency magnetron sputtering of substituted β-tricalcium phosphate targets",
abstract = "The influence of magnesium and/or strontium substitutions on the deposition rate of P-TCP was investigated. Pure β-TCP, Mg-β-TCP, Sr-β-TCP and Mg/Sr-β-TCP targets were used for the coating formation. It was shown that strontium substitutions in the structure of β-TCP target increase the deposition rate of coatings. Magnesium substitutions, on the contrary, decrease this parameter. It makes it possible to increase the deposition rate of coatings formed by radio frequency magnetron sputtering without any negative effect on coatings properties. It was demonstrated that all coatings formed by radio frequency magnetron sputtering of β-TCP targets were calcium-rich. The methods of AFM and SEM revealed that coatings under study were characterized by various morphologies. Magnesium-containing coatings (Mg-β-TCP and Mg/Sr-β-TCP) had the lower value of nanohardness than other ones. All coatings were characterized by the higher value of surface free energy than titanium substrate. The coatings formed by sputtering of β-TCP, Mg-β-TCP, Sr-β-TCP had approximately the same value of this parameter.",
author = "Fedotkin, {A. Y.} and Bolbasov, {E. N.} and Kozelskaya, {A. I.} and Useinov, {A. S.} and Tverdokhlebov, {S. I.}",
year = "2018",
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T1 - Deposition of calcium phosphate coatings using radio frequency magnetron sputtering of substituted β-tricalcium phosphate targets

AU - Fedotkin, A. Y.

AU - Bolbasov, E. N.

AU - Kozelskaya, A. I.

AU - Useinov, A. S.

AU - Tverdokhlebov, S. I.

PY - 2018/11/27

Y1 - 2018/11/27

N2 - The influence of magnesium and/or strontium substitutions on the deposition rate of P-TCP was investigated. Pure β-TCP, Mg-β-TCP, Sr-β-TCP and Mg/Sr-β-TCP targets were used for the coating formation. It was shown that strontium substitutions in the structure of β-TCP target increase the deposition rate of coatings. Magnesium substitutions, on the contrary, decrease this parameter. It makes it possible to increase the deposition rate of coatings formed by radio frequency magnetron sputtering without any negative effect on coatings properties. It was demonstrated that all coatings formed by radio frequency magnetron sputtering of β-TCP targets were calcium-rich. The methods of AFM and SEM revealed that coatings under study were characterized by various morphologies. Magnesium-containing coatings (Mg-β-TCP and Mg/Sr-β-TCP) had the lower value of nanohardness than other ones. All coatings were characterized by the higher value of surface free energy than titanium substrate. The coatings formed by sputtering of β-TCP, Mg-β-TCP, Sr-β-TCP had approximately the same value of this parameter.

AB - The influence of magnesium and/or strontium substitutions on the deposition rate of P-TCP was investigated. Pure β-TCP, Mg-β-TCP, Sr-β-TCP and Mg/Sr-β-TCP targets were used for the coating formation. It was shown that strontium substitutions in the structure of β-TCP target increase the deposition rate of coatings. Magnesium substitutions, on the contrary, decrease this parameter. It makes it possible to increase the deposition rate of coatings formed by radio frequency magnetron sputtering without any negative effect on coatings properties. It was demonstrated that all coatings formed by radio frequency magnetron sputtering of β-TCP targets were calcium-rich. The methods of AFM and SEM revealed that coatings under study were characterized by various morphologies. Magnesium-containing coatings (Mg-β-TCP and Mg/Sr-β-TCP) had the lower value of nanohardness than other ones. All coatings were characterized by the higher value of surface free energy than titanium substrate. The coatings formed by sputtering of β-TCP, Mg-β-TCP, Sr-β-TCP had approximately the same value of this parameter.

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