Abstract
LiFe5O8 solid-phase synthesis at radiation-thermal (RT) annealing of lithium carbonate and iron oxide mechanical mixture was studied using thermal analysis (TG/DSC) and X-ray powder diffraction (XRD) techniques. The RT annealing was proceeded with high-power pulsing beam of 2.4 MeV electrons. It was shown that RT synthesis of the precursors considerably enhances the reactivity of the solid system within temperatures range 600-800 °C. In particular, lithium ferrite can be obtained at lower temperatures than those necessary in the absence of RT annealing.
Original language | English |
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Pages (from-to) | 11-13 |
Number of pages | 3 |
Journal | Journal of Thermal Analysis and Calorimetry |
Volume | 101 |
Issue number | 1 |
DOIs | |
Publication status | Published - Jul 2010 |
Keywords
- DSC
- Ferrite
- Kinetics
- LiFeO formation
- Radiation-thermal synthesis
- TG
ASJC Scopus subject areas
- Physical and Theoretical Chemistry
- Condensed Matter Physics