Analytical control of lactide synthesis

Daria S. Krutas, Margarita K. Zamanova, Aleksandr E. Lukianov, Aleksey L. Zinovyev, Viktor T. Novikov, Tatyana N. Volgina

Research output: Contribution to journalArticle

1 Citation (Scopus)

Abstract

The technique of identification and quantification of D,L-lactide, lactic acid and its oligomers by the method of high performance liquid chromatography (HPLC) was developed. The separation was done on two columns connected consecutively using an aqueous solution of orthophosphoric acid and acetonitrile in the ratio 88:12 vol. % at a flow rate of 1.2 ml min-1 as a mobile phase. The developed method is simple and linear. Research of specificity, accuracy, repeatability and reproducibility shows that the technique is suitable for analytical control of all stages of the lactide synthesis from lactic acid.

Original languageEnglish
Pages (from-to)567-572
Number of pages6
JournalPetroleum and Coal
Volume58
Issue number5
Publication statusPublished - 1 Jan 2016

Fingerprint

Lactic acid
Orthophosphoric acid
High performance liquid chromatography
Acetonitrile
Oligomers
Flow rate

Keywords

  • Analysis lactide
  • Chromatography
  • Lactic acid
  • Lactide
  • Oligomer

ASJC Scopus subject areas

  • Energy(all)

Cite this

Krutas, D. S., Zamanova, M. K., Lukianov, A. E., Zinovyev, A. L., Novikov, V. T., & Volgina, T. N. (2016). Analytical control of lactide synthesis. Petroleum and Coal, 58(5), 567-572.

Analytical control of lactide synthesis. / Krutas, Daria S.; Zamanova, Margarita K.; Lukianov, Aleksandr E.; Zinovyev, Aleksey L.; Novikov, Viktor T.; Volgina, Tatyana N.

In: Petroleum and Coal, Vol. 58, No. 5, 01.01.2016, p. 567-572.

Research output: Contribution to journalArticle

Krutas, DS, Zamanova, MK, Lukianov, AE, Zinovyev, AL, Novikov, VT & Volgina, TN 2016, 'Analytical control of lactide synthesis', Petroleum and Coal, vol. 58, no. 5, pp. 567-572.
Krutas DS, Zamanova MK, Lukianov AE, Zinovyev AL, Novikov VT, Volgina TN. Analytical control of lactide synthesis. Petroleum and Coal. 2016 Jan 1;58(5):567-572.
Krutas, Daria S. ; Zamanova, Margarita K. ; Lukianov, Aleksandr E. ; Zinovyev, Aleksey L. ; Novikov, Viktor T. ; Volgina, Tatyana N. / Analytical control of lactide synthesis. In: Petroleum and Coal. 2016 ; Vol. 58, No. 5. pp. 567-572.
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