Adhesion properties of a silicon-containing calcium phosphate coating deposited by RF magnetron sputtering on a heated substrate

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10 Citations (Scopus)

Abstract

Silicon-containing hydroxyapatite coatings 400-700 nm in thickness are prepared by means of radio-frequency (RF) magnetron sputtering on a heated (to 200°C) titanium substrate chemically etched and treated with a pulsed electron beam. The morphology and phase composition of the coating are studied. The morphology and roughness of the composite "calcium-phosphate coating-titanium substrate" differ depending on the treatment procedure of the substrate before deposition. The scratch test method is used to assess the adhesion strength of the coatings formed at different values of bias potential applied to the substrate. It is observed that the adhesion strength of the coating changes with decreasing crystallite size.

Original languageEnglish
Pages (from-to)944-951
Number of pages8
JournalJournal of Surface Investigation
Volume7
Issue number5
DOIs
Publication statusPublished - 1 Sep 2013

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Phosphate coatings
Calcium phosphate
Silicon
Magnetron sputtering
Adhesion
Coatings
Bond strength (materials)
Substrates
Titanium
Crystallite size
Hydroxyapatite
Phase composition
Electron beams
Durapatite
Surface roughness
calcium phosphate
Composite materials

ASJC Scopus subject areas

  • Surfaces, Coatings and Films

Cite this

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title = "Adhesion properties of a silicon-containing calcium phosphate coating deposited by RF magnetron sputtering on a heated substrate",
abstract = "Silicon-containing hydroxyapatite coatings 400-700 nm in thickness are prepared by means of radio-frequency (RF) magnetron sputtering on a heated (to 200°C) titanium substrate chemically etched and treated with a pulsed electron beam. The morphology and phase composition of the coating are studied. The morphology and roughness of the composite {"}calcium-phosphate coating-titanium substrate{"} differ depending on the treatment procedure of the substrate before deposition. The scratch test method is used to assess the adhesion strength of the coatings formed at different values of bias potential applied to the substrate. It is observed that the adhesion strength of the coating changes with decreasing crystallite size.",
author = "Surmeneva, {M. A.} and Surmenev, {R. A.} and Pichugin, {V. F.} and Koval, {Nikolay Nikolaevich} and Teresov, {A. D.} and Ivanova, {A. A.} and Grubova, {I. Yu} and Ignatov, {Victor Pavlovich} and O. Primak and M. Epple",
year = "2013",
month = "9",
day = "1",
doi = "10.1134/S102745101305039X",
language = "English",
volume = "7",
pages = "944--951",
journal = "Journal of Surface Investigation",
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publisher = "Maik Nauka-Interperiodica Publishing",
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TY - JOUR

T1 - Adhesion properties of a silicon-containing calcium phosphate coating deposited by RF magnetron sputtering on a heated substrate

AU - Surmeneva, M. A.

AU - Surmenev, R. A.

AU - Pichugin, V. F.

AU - Koval, Nikolay Nikolaevich

AU - Teresov, A. D.

AU - Ivanova, A. A.

AU - Grubova, I. Yu

AU - Ignatov, Victor Pavlovich

AU - Primak, O.

AU - Epple, M.

PY - 2013/9/1

Y1 - 2013/9/1

N2 - Silicon-containing hydroxyapatite coatings 400-700 nm in thickness are prepared by means of radio-frequency (RF) magnetron sputtering on a heated (to 200°C) titanium substrate chemically etched and treated with a pulsed electron beam. The morphology and phase composition of the coating are studied. The morphology and roughness of the composite "calcium-phosphate coating-titanium substrate" differ depending on the treatment procedure of the substrate before deposition. The scratch test method is used to assess the adhesion strength of the coatings formed at different values of bias potential applied to the substrate. It is observed that the adhesion strength of the coating changes with decreasing crystallite size.

AB - Silicon-containing hydroxyapatite coatings 400-700 nm in thickness are prepared by means of radio-frequency (RF) magnetron sputtering on a heated (to 200°C) titanium substrate chemically etched and treated with a pulsed electron beam. The morphology and phase composition of the coating are studied. The morphology and roughness of the composite "calcium-phosphate coating-titanium substrate" differ depending on the treatment procedure of the substrate before deposition. The scratch test method is used to assess the adhesion strength of the coatings formed at different values of bias potential applied to the substrate. It is observed that the adhesion strength of the coating changes with decreasing crystallite size.

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